Methods of reducing the body weight of a subject by administering a fatty acid ester of an estrogen or estrogen derivative in an oil and compositions containing the same
a technology of fatty acid ester and body weight, which is applied in the field of compositions and methods of reducing the body weight of a subject, can solve the problems of limited success, difficulty in all these approaches, and limited room for external manipulation, so as to reduce body weight, reduce body weight, and reduce body weigh
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example 1
[0052]An oil evaluation was done to determine the solubility behavior of oleoyl-estrone as a function of type of oil, concentration and temperature. The solubility of oleoyl-estrone was evaluated at concentrations of 60 mg / g and 200 mg / g. For the 60 mg / g solutions, the solubility was observed for 96 hours at room temperature, then the temperature was cycled to 5° C. for 96 hours, after which the solution was returned to room temperature. For the 200 mg / g solutions, the solubility was observed for 96 hours at 40° C., then the temperature was cycled to room temperature for 24 hours, then stored at 5° C. for 96 hours before being returned to room temperature. Table 1 and Table 2 show the oils tested and the test results.
TABLE 160 mg / g of Oleoyl-Estrone in Oil at RoomTemperature (RT) (about 22° C.)Cycledto 5° C.OilAfter 24 hrAfter 96 hrafter 96 hrCanolaDissolvedDissolvedDissolvedLabrasolDissolvedDissolvedPrecipitatedafter 4 hrLabrafil M 125CSNOTNOT Dissolved more oilDissolvedDissolvedad...
example 2
[0054]The compatibility of oleoyl-estrone in various oil systems was also assessed. The respective stability of oleoyl-estrone in various oils was assessed following storage at (A) 25° C. / 60% and relative humidity (RH), (B) 40° C. / 75% RH, (C) 50° C. and (D) 60° C. in canola oil, safflower oil, Captex and a 2:1 Captex: Labrafil mixture. The stability test methods include appearance / color, potency, and related substances (e.g. impurities or degradant in the oleoyl-estrone and oil mixture). The results of the three week tests are set forth in Tables 4-7.
TABLE 4Time ZeroOne WeekTwo WeeksAnalysisCANOLACANOLACANOLAConditionN / A25° C. / 60%40° C. / 75%50° C.60° C.25° C. / 60%40° C. / 75%RHRHRHRHPull DateN / A11 AUG 0411 AUG 0411 AUG 0411 AUG 0418 AUG 0418 AUG 04Assay Date04 AUG 0411 AUG 0411 AUG 0411 AUG 0411 AUG 0418 AUG 0418 AUG 04Appearance / Clear andClear andClear andClear andClear andClear andClear andColorpale yellowpale yellowpale yellowpale yellowpale yellowpale yellowpale yellowReference Std ...
example 3
[0057]Capsules containing 1 mg, 10 mg and 50 mg of oleoyl-estrone are prepared according to the formulations shown in Table 8 and according the method shown in FIG. 1.
TABLE 8Amount of Component per BatchComponent1 mg capsule10 mg capsule50 mg capsuleOleoyl-Estrone1.160 g14.0 g72.50 gSafflower Oil56.84 g98.0 g507.5 gTotal58.00 g112.0 g 580.0 g
[0058]FIG. 1 is a flow diagram that illustrates the manufacturing process of making the oleoyl-estrone capsules as discussed herein. Each of the three batch formulations were manufactured by dissolving the indicated amount of oleoyl-estrone in safflower oil (Step A of FIG. 1). To facilitate dissolution, heat was applied to maintain a temperature of 40° C. Then gelatin capsules are filled with each batch of oleoyl-estrone and safflower oil and then placed upright in a capsule holder (Step B of FIG. 1). The fill weights of the 1 mg, 10 mg, and 50 mg dosage strength capsules are provided in Table 9.
TABLE 9Dosage (mg)Capsule Fill Weight (mg) ± 5%150...
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