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Device and method for separating pressized nitrogen gas from air

An air separation and pressure technology, applied in the direction of nitrogen purification/separation, can solve the problems of increasing and failing to further reduce the energy consumption of nitrogen production, and achieve the effect of improving the extraction rate, reducing energy consumption, and reducing the height of the cold box

Active Publication Date: 2010-01-20
SHANGHAI QIYUAN GAS DEV
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  • Abstract
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  • Claims
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Problems solved by technology

The double-tower nitrogen waste gas expansion refrigeration (double-tower reflux) process increases the oxygen content of the liquid air entering the low-pressure tower through the high-pressure tower purification, but because the heat source of the low-pressure tower reboiler is nitrogen at the top of the high-pressure tower, the high-pressure tower The pressure is increased due to the heat transfer temperature difference, so that the energy consumption of nitrogen production cannot be further reduced

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  • Device and method for separating pressized nitrogen gas from air

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Embodiment Construction

[0027] see figure 1 , the device for producing pressure nitrogen by air separation of the present invention includes a pressurized turboexpander 1, an air cooler 2, a main heat exchanger 3, a low pressure tower 4, a reboiler 5 arranged in the low pressure tower, and a low pressure tower. Condensing evaporator 6, high pressure tower 7, high pressure tower condensing evaporator 8 and subcooler 9. The low pressure column 4 and the high pressure column 7 are arranged side by side in the same cold box.

[0028] The inlet of the supercharging end 11 of the supercharged turboexpander 1 is connected to the first raw material air pipeline 101 , the outlet is connected to the raw material air inlet 21 of the air cooler 2 , and the raw material air outlet 22 of the air cooler is connected to the first raw material air pipeline 101 of the main heat exchanger 3 . A feed air inlet 31, the first feed air outlet 32 ​​of the main heat exchanger is connected to the inlet of the expansion end 1...

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Abstract

The invention relates to a device separating the air to produce the pressurized nitrogen, and comprises a pressurized turbine inflation machine, an air cooler, a main heat exchanger, a low-pressure tower, a re-boiler that is arranged inside the low-pressure tower, a low-pressure tower condensation evaporator, a high-pressure tower, a high-pressure tower condensation evaporator and a sub-cooler, wherein, the low-pressure tower and the high-pressure tower are arranged in the same cooling box side by side. Each device is connected with each other through a connection pipe. The invention relates to a method for separating the air to produce the pressurized nitrogen, which adopts the following steps: the raw material air enters into the pressurized turbine inflation machine to be inflated and cooled, and flows into the low-pressure tower to be rectified and separated, so that the high-pressure nitrogen can be obtained at the top of the high-pressure tower and is adopted as the finished product to be outputted. Adopting the device and the method, the nitrogen extraction rate can reach 78 to 86 percent; compared with the single-tower air inflation nitrogen production, the electricity consumption of the unit product can be reduced by 17 percent; compared with the dual-tower waste-gas inflation refrigeration flowing procedure (dual-tower return flow), the electricity consumption can be reduced by 10 to 15 percent.

Description

technical field [0001] The invention relates to a gas separation device and a separation method, in particular to a device and method for preparing pressure nitrogen by air separation. Background technique [0002] In the production process of float glass, a large amount of nitrogen needs to be used as protective gas, the gas pressure is 0.15-0.4MPa, and the nitrogen purity is less than or equal to 3ppmO 2 . At the same time, a small amount of liquid nitrogen (≤5% nitrogen production) is required for backup. Therefore, in float glass production enterprises, a device for producing pressure nitrogen by air separation is generally attached. A device for producing pressure nitrogen by air separation in the prior art adopts single tower reflux oxygen-rich (waste gas) expansion to produce nitrogen, and its energy consumption is 0.28-0.35KWh / NM. 3 N 2 . Another device for producing pressure nitrogen by air separation is to use air expansion single tower to produce nitrogen. Th...

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B21/04
Inventor 周大荣俞建
Owner SHANGHAI QIYUAN GAS DEV