Method for producing epoxy plasticizer using waste grease

A technology of epoxy plasticizer and waste oil, which is applied in the production of plasticizers, and uses waste oil to produce epoxy plasticizers. It can reduce the harm to the environment and people's health, improve flexibility, and have a wide range of effects.

Inactive Publication Date: 2007-11-14
江苏向阳科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

Inventions described in this patents involve making new materials from recycled or reused oils that have specific qualities such as being cheaply available at reasonable prices, easy to produce with minimal emissions during manufacturing processes, good thermal properties (low volatility), high reactivity towards chemical agents like amines) without requiring expensive acids or other substances added. These novel compounds may be useful in various industries including plastisol coatings, adhesives, paints, printing fluids, lubricants, etc., where they provide improved performance over existing alternatives due to their unique physical attributes.

Problems solved by technology

The technical problem addressed in this patented text relating to current plastifier compositions used worldwide that contains chlorinated organics like Phthaquinone®(BPA). These substances can be dangerous even at low concentrations but it has been found that these plasterifiers could still pose environmental concerns due to their potential negative impact upon human health. There exists an urgent need for improved plasma resins made from renewables instead of fossil fuel sources with reduced levels of certain components without compromising safety standards.

Method used

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  • Method for producing epoxy plasticizer using waste grease
  • Method for producing epoxy plasticizer using waste grease
  • Method for producing epoxy plasticizer using waste grease

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Embodiment 1: the waste oil is heated to 45 ℃ and filtered through a filter press to remove solid particles to obtain hot oil, add 3~6% sodium hydroxide solution to the hot oil, fully stir and then extract and separate and remove fatty acid sodium and colloid, take a sample When the acid value (KOHmg / g) is less than 1.0 by analysis and determination, carry out vacuum distillation, dehydration and deodorization, and at -0.05MPa, heat to 80 ° C until the water evaporates and remove the peculiar smell at the same time; then use activated clay for adsorption and decolorization (with Activated clay is 1 part, 30 parts of fats and oils are fed in proportions), and the activated clay is recycled and reused, and the glycerides obtained are pumped into the transesterification kettle, and the weight ratio of glycerides, methanol and sodium hydroxide is: 1: (0.20 ~0.24): (0.00036~0.00044) feed intake, heat and stir, react 2 hours under reflux state; After the reaction finishes, thi...

Embodiment 2

[0027] Embodiment 2: the basic catalyst used in the transesterification process is potassium hydroxide, and other technical parameters and operation steps are the same as those in the embodiment, to obtain the epoxy fatty acid methyl ester finished product.

Embodiment 3

[0028] Example 3: For organic acid, acetic acid was used instead of formic acid, and other technical parameters and operation steps were the same as those in Example 1 to obtain the finished epoxy plasticizer.

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Abstract

This invention relates to one kind of method to use abandoned grease to produce epoxy plasticizer, its characteristic lies in: Use the abandoned grease as raw materials, by pretreatment, the obtained glycerin ester to ester exchange respond with the methyl alcohol under alkali catalysis, then get fatty acidmethyl ester, then again with the peroxide organic acid, which is the reaction products of hydrogen peroxide and organic acid, to directly epoxy respond, get the raw epoxy fatty acid methyl ester, then wash off the acid by water, and obtain the epoxy fatty acid methyl ester by distillation and dehydration product. The raw material cost of this invention is low, originates broadly, conforms to the green environmental protection requirement, and the craft is simple, does not pollute environment, so it is the good substitute of petroleum product.

Description

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Claims

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Application Information

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Owner 江苏向阳科技有限公司
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