Fused pyrazole derivatives and uses of methods of treatment of metabolic-related disorders thereof
A technology of compounds and hydrates, applied in the field of treatment of metabolic-related disorders including the following disorders, can solve the problems of inability to identify nicotinic acid receptors, obstacles and the like
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0471] Will 125 Synthetic methods for incorporating activity levels of I into target molecules include:
[0472] A. Sandmeyer and its analogs - This procedure converts an aryl or heteroaryl amine to a diazonium salt such as tetrafluoroborate, and then uses Na 125 I convert it into 125 I labeled compound. A representative procedure is reported by Zhu, D.-G. and co-workers in J. Org. Chem. 2002, 67, 943-948.
[0473] B. o 125 Phenol I - This procedure allows incorporation at the ortho position of the phenol 125 I, as reported by Collier, T.L. and coworkers in J. Labeled Compd Radiopharm. 1999, 42, S264-S266.
[0474] C. Aryl and heteroaryl bromides with 125 I Exchange - This method is usually a two-step process. The first step is to use (for example) Pd to catalyze the reaction [ie Pd(Ph 3 P) 4 ] or via an aryl or heteroaryl lithium in a trialkyltin halide or hexaalkylditin [e.g., (CH 3 ) 3 SnSn(CH 3 ) 3 ], the aryl or heteroaryl bromide is converted to the correspo...
example
[0480] The following examples are provided for illustrative purposes and not by way of limitation. Based on the disclosure herein, one of ordinary skill in the art will be able to devise equivalent assays and methods, all of which form a part of the present invention.
example 1
[0482] Rodent Diabetic Models
[0483] Rodent models of type 2 diabetes associated with obesity and insulin resistance have been developed. To understand the pathophysiology of disease and to test candidate therapeutic compounds, genetic models such as db / db and ob / ob in mice [see Diabetes (1982) 31:1-6] and fa / fa in zucker rats have been developed [ Diabetes (1983) 32:830-838; Annu Rep Sankyo Res Lab (1994) 46:1-57]. The homozygous animal C57BL / KsJ-db / db mouse developed by Jackson Laboratory (Jackson Laboratory) is a mouse with obesity, hyperglycemia, insulin hypersecretion and insulin resistance [J Clin Invest (1990) 85: 962-967 ], while heterozygotes are lean and normoglycemic. In the db / db model, mice progressively develop insulin deficiency with age, a feature commonly observed in advanced stages of human type 2 diabetes when glucose levels are not adequately controlled. Since this model is similar to the human type 2 diabetes model, the compounds of the invention were...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More 