Nano silver antimicrobial solution and preparing method thereof
A technology of nano-silver antibacterial and nano-metallic silver, which is applied in botany equipment and methods, chemicals for biological control, animal repellants, etc. Stability and other issues, to achieve the effect of simple preparation method, uniform distribution, and increased stability
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Embodiment 1
[0012] In the deionized aqueous solution containing 0.001mmol / L nano-metallic silver particles and 0.01mol / L carboxymethyl chitosan, add hydrazine hydrate reducing agent with 2 times the molar concentration of silver ion at 60°C, and react for 0.5h under stirring. The nano-silver antibacterial solution containing 0.001mol / L nano-metal silver particles (with a particle diameter of 3nm) and 0.01mmol / L carboxymethyl chitosan can be obtained.
Embodiment 2
[0014] In the deionized aqueous solution containing 0.008mmol / L nano-metallic silver particles and 0.02mmol / L carboxymethyl chitosan, add hydrazine hydrate reducing agent with 2 times the molar concentration of silver ion at 50°C, and react for 2 hours under stirring Obtain the nano-silver antibacterial solution containing 0.02mmol / L nano-metallic silver particles (particle diameter is 11nm) and 0.008mmol / L carboxymethyl chitosan.
Embodiment 3
[0016] Add hydrazine hydrate reducing agent with 2 times the molar concentration of silver ion to the deionized aqueous solution containing 0.02mmol / L nano-metallic silver particles and 0.05mmol / L carboxymethyl chitosan at 30°C, and react for 3h under stirring The nano-silver antibacterial solution containing 0.02mmol / L nano-metal silver particles (with a particle diameter of 30nm) and 0.02mmol / L carboxymethyl chitosan can be obtained.
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