Base specific cleavage of methylation-specific amplification products in combination with mass analysis
A technology of amplification products and methylation, which is used in the determination/inspection of microorganisms, biochemical equipment and methods, fermentation, etc., and can solve the problems of labor consumption and a large amount of high-quality genomic DNA.
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Embodiment I
[0650] The following example illustrates a method for identifying the molecular methylation status of a target nucleic acid molecule.
[0651] method
[0652] bisulfite treatment
[0653] Bisulfite treatment was performed according to the method given in Paulin et al. Nucl. Acids Res. 26:5009-5011 (1998). Genomic DNA (2 μg) was digested with restriction endonucleases, then denatured by adding 3M sodium hydroxide and incubated at 37°C for 15 min. Add 6.24M urea / 2M meta-bisulfite (4M bisulfite) solution and 10mM sodium hydroquinone solution to the denatured DNA to achieve the final concentration: 5.36M urea, 3.44M bisulfite, 0.5 mM hydroquinone. The DNA solution was placed in a 0.5 ml tube and covered with mineral oil, and 20 cycles were performed in a PCR machine, with the tube repeatedly heated to 95°C for 30 seconds and incubated at 55°C for 15 min. In addition to desalting the DNA using a Bresaclean DNA purification procedure (Geneworks, Adelaide, Australia), the bisulfi...
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