Black dye composition and black ink composition
一种黑色染料、组成物的技术,应用在有机染料、油墨、颜料浆料等方向,能够解决日光牢度等特性不佳、未能满足打印需求、墨水pH值不稳定等问题
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preparation example 1
[0164] Take 300 parts of the compound of formula (I-2), add 2700 parts of water to adjust the dissolution, adjust the pH value to 10-11 with 45% aqueous sodium hydroxide solution, and control the temperature at 80-85 ° C, carry out the hydrolysis reaction for 90 minutes, and then use 32 % hydrochloric acid solution to adjust the pH value to 5-9, perform reverse osmosis desalination, and spray dry to obtain the compound of formula (I-1) of the present invention.
[0165]
preparation example 2
[0167] The compound of formula (II-1) of the present invention can be obtained by using the compound of formula (II-2) as a starting material and repeating the steps of Preparation 1.
[0168]
preparation example 3
[0170] The compound of formula (IV-1) of the present invention can be obtained by using the compound of formula (IV-2) as a starting material and repeating the steps of Preparation 1.
[0171]
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