Method for preparing bamboo dissolving pulp by improved prehydrolysis alkaline process and product thereof
A technology of dissolving pulp and pre-hydrolysis, which is applied in pulping with inorganic alkali, pretreatment with acidic compounds, non-woody plant/crop pulp, etc., can solve the problems of process shortening and waste of resources, and achieve the reduction of processing costs and comprehensive The effect of low production cost
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Examples
Embodiment 1
[0066] Provide a kind of method that the improved pre-hydrolysis alkali method manufactures bamboo dissolving pulp, comprises the steps:
[0067] (1) Bamboo material preparation: cut two to three-year-old bamboo into bamboo chips with a length of 15-30mm, a width of 10-20mm, and a thickness of 3-8mm through a slicer, screen through a high-frequency vibrating screen, and spray and wash with high-pressure water , remove impurities and dust;
[0068] (2) Pretreatment: carried out in a hydrolysis pot, the treatment agent is sulfuric acid, and the process conditions are: the sulfuric acid concentration is 0.1wt%, the temperature is 110 ° C, the liquid ratio is 1: 10, the treatment time is 60 minutes, and the treatment is discharged after the pretreatment liquid, and washing material;
[0069] (3) Pre-hydrolysis: carried out in a hydrolysis pot, the hydrolysis catalyst is sulfuric acid, and the process conditions are: the concentration of sulfuric acid is 0.7wt%, the temperature is...
Embodiment 2
[0081] Provide another kind of improved prehydrolysis alkali method to manufacture the method for bamboo dissolving pulp, comprise the steps:
[0082] (1) Bamboo material preparation: with embodiment 1, two to three-year-old bamboo materials are cut into long 15~30mm, wide 10~20mm, thick 3~8mm bamboo slices by slicer, screened by high-frequency vibrating sieve, and use high-pressure Spray washing with water to remove impurities and dust;
[0083] (2) pretreatment: with embodiment 1, carry out in hydrolysis pot, treatment agent is sulfuric acid, and process condition is: sulfuric acid concentration is 0.1wt%, and temperature is 110 ℃, and liquid ratio is 1: 10, and treatment time is 60 minutes, After pretreatment, the treatment liquid is discharged and the material is washed;
[0084] (3) Pre-hydrolysis: carried out in a hydrolysis pot, the hydrolysis catalyst is sulfuric acid, the process conditions are: the acid concentration is 1.5wt%, the temperature is 125 ° C, the liquid...
Embodiment 3
[0087] Provide another kind of improved prehydrolysis alkali method to manufacture the method for bamboo dissolving pulp, comprise the steps:
[0088] (1) Bamboo material preparation: with embodiment 1, two to three-year-old bamboo materials are cut into long 15~30mm, wide 10~20mm, thick 3~8mm bamboo slices by slicer, screened by high-frequency vibrating sieve, and use high-pressure Spray washing with water to remove impurities and dust;
[0089] (2) pretreatment: with embodiment 1, carry out in hydrolysis pot, treatment agent is sulfuric acid, and technological condition is: sulfuric acid concentration is 0.1wt%, and temperature is 110 ℃, and liquid ratio is 1: 10, and treatment time is 60 minutes, After pretreatment, the treatment liquid is discharged and the material is washed;
[0090] (3) pre-hydrolysis: with embodiment 1, carry out in hydrolysis pot, hydrolysis catalyst is sulfuric acid, and process condition is: sulfuric acid concentration is 0.7wt%, and temperature is...
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Abstract
Description
Claims
Application Information
- IPC
- D21C1/04; D21C3/02; D21H11/12
- Inventors
- 吴学东; 陈惠敏
