The application belongs to the technical field of rubber additive synthesis, and particularly relates to a method for continuously preparing 4,4'-
dithiodimorpholine. The method uses
sulfur monochloride,
morpholine, 32wt% liquid alkali (
sodium hydroxide solution) and 120#
solvent oil as raw materials, and generates 4,4'-
dithiodimorpholine in a dynamic tubular reactor. After the reaction is completed, the material flowing out of the dynamic tubular reactor is collected, and the product is obtained through static layering, washing, filtering and
drying. The method uses the dynamic tubular reactor for reaction, and the
mass transfer and
heat transfer efficiency are extremely high. The material is instantaneously and uniformly mixed, so that the
morpholine and the
sulfur monochloride are rapidly contacted and reacted, the reaction heat can be instantaneously removed, the optimal
reaction temperature can be accurately maintained, the
continuous production can be realized, the production capacity is greatly improved, the reaction time of the traditional kettle reactor is shortened from 2-7h to 10min, the
raw material conversion rate is as high as 99% or more, and the goals of cost reduction and efficiency improvement, green safety are finally achieved.