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Device for preparing carbon nano tube by arc process

A carbon nanotube and arc method technology, which is applied to the device field in the field of nanotechnology, can solve the problems of amorphous carbon and other impurities, the purity of carbon nanotubes is not high, and the purity of products is reduced, so as to achieve a suitable growth environment and optimize growth. conditions, the effect of improving the purity

Inactive Publication Date: 2010-02-24
SHANGHAI JIAO TONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the continuous arc reaction, the impurities such as amorphous carbon attached to the previously formed carbon nanotube network product will reduce the purity of the product, so that the prepared carbon nanotubes are not high in purity, and impurities such as amorphous carbon Obviously, the device involved in this utility model cannot solve this problem

Method used

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  • Device for preparing carbon nano tube by arc process
  • Device for preparing carbon nano tube by arc process
  • Device for preparing carbon nano tube by arc process

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] The preparation device of this embodiment is as image 3 As shown, it includes: cathode graphite rod 1, anode graphite rod 2, scraper 3, thermocouple 5, collection turntable 6, drive motor 7, fixed graphite disk 8, reaction chamber 9, carbon nanotube collection box 10, anode graphite Rod propulsion device 11, air inlet 12, air extraction port 13, wherein, anode graphite rod 2 diameters are 6mm, long 80mm; Anode graphite rod 2 contains Ni / Co / Fe catalyst (the mass ratio of Ni: Co: Fe 5: 1 : 1, graphite accounts for 95% of the total mass of the anode graphite rod); the anode graphite rod 2 is fixed on the anode graphite rod propelling device 11; the cathode graphite rod 1 is a high-purity graphite rod, and its diameter is 8mm, and the length is 300mm; the anode graphite rod It is arranged opposite to the cathode graphite rod, leaving a distance of 3 mm in the middle; the fixed graphite disc 8 is located 40 mm below the anode graphite rod 2 and the cathode graphite rod 1; ...

Embodiment 2

[0029] The preparation device of this embodiment includes: cathode graphite rod 1, anode graphite rod 2, reaction chamber 9, anode graphite rod propelling device 11, air inlet 12, air extraction port 13, scraper 3, thermocouple 5, collection turntable 6. Drive motor 7, carbon nanotube collection box 10. Among them, the anode graphite rod 2 has a diameter of 6 mm and a length of 80 mm; the anode graphite rod 2 is made of Ni, Y 2 o 3 , graphite powder as raw material (Ni and Y 2 o 3The role of catalyst), according to the molar ratio of Ni: Y: C is 4.2: 1: 94.8 to carry out batching, after mixing uniformly press rod molding; Anode graphite rod 2 is fixed on the anode graphite rod propelling device 11; Cathode graphite rod 1 It is a high-purity graphite rod with a diameter of 8 mm and a length of 300 mm; the anode graphite rod and the cathode graphite rod are arranged opposite to each other, leaving a distance of 2 mm in the middle; Cut, the carbon nanotube collection box 10 i...

Embodiment 3

[0036] The preparation device of this embodiment includes: cathode graphite rod 1, anode graphite rod 2, reaction chamber 9, anode graphite rod propelling device 11, air inlet 12, air extraction port 13, scraper 3, thermocouple 5, collection turntable 6. Drive motor 7, carbon nanotube collection box 10. Among them, the anode graphite rod 2 has a diameter of 6 mm and a length of 80 mm; the anode graphite rod 2 is made of Ni, Y 2 o 3 , CeO 2 , graphite powder as raw material (Ni, Y 2 o 3 , CeO 2 The role of catalyst), according to the molar ratio of Ni: Y: Ce: C is 4.2: 1: 0.1: 94.7 to carry out the batching, after mixing evenly, the rod is formed; the anode graphite rod 2 is fixed on the anode graphite rod propulsion device 11; The cathode graphite rod 1 is a high-purity graphite rod with a diameter of 8mm and a length of 300mm; the anode graphite rod and the cathode graphite rod are arranged opposite to each other, leaving a distance of 2mm in the middle; the collection t...

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Abstract

The invention relates to a device for preparing a carbon nano tube by an arc process in the nano technical field. The device comprises a cathode graphite rod, an anode graphite rod, a reaction cavity,an anode graphite rod propelling device, an air inlet, an extraction opening, a scraping plate, a thermocouple, a collecting turntable, a drive motor and a carbon nano tube collecting box, wherein the anode graphite rod is fixed on the anode graphite rod propelling device and is arranged opposite to the cathode graphite rod, and a clearance is remained between the cathode graphite rod and the anode graphite rod; the collecting turntable is connected with the drive motor, the scraping plate is tangential to the collecting surface of the collecting turntable, the carbon nano tube collecting boxis arranged under the collecting turntable, and the thermocouple and the drive motor are fixed on the reaction cavity; and the air inlet and the extraction opening are arranged on the reaction cavity. The device enables the carbon nano tube to grow on the collecting turntable by keeping a relatively stable temperature, also enables the growing carbon nano tube not to absorb amorphous carbon, andother impurities generated later and further improves the purity of the prepared carbon nano tube.

Description

technical field [0001] The invention relates to a device in the field of nanotechnology, in particular to a device for preparing carbon nanotubes by an arc method. Background technique [0002] Since the discovery of carbon nanotubes (CNTs) in 1991, due to their excellent mechanical properties and adjustable electrical properties, carbon nanotubes have been widely used in nanoelectronic devices, field emission technology, biological drug loading, and hydrogen storage technology. And many other fields have significant application potential. Carbon nanotubes can be divided into single-wall carbon nanotubes (SWNT), double-wall carbon nanotubes (DWNT), and multi-wall carbon nanotubes (MWNT). Among them, single-wall carbon nanotubes, as excellent one-dimensional nanomaterials, are used to manufacture nanoelectronic devices such as field effect transistors and thin film transistors because of their high carrier mobility. They are expected to replace silicon materials and become t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B31/02B82B3/00
Inventor 张亚非苏言杰魏浩
Owner SHANGHAI JIAO TONG UNIV
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