Method for preparing low-temperature cured conductive paste
A conductive paste, low temperature technology, used in conductive materials, conductive materials, cable/conductor manufacturing, etc., can solve the problems of high price and high cost in the electronic market, and achieve the effect of reducing production costs
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[0018] The invention discloses a preparation method of sheet low-temperature curing conductive paste, which comprises the following steps:
[0019] Step 1): Preparation of organic vehicle
[0020] Dissolve one or more of 10.0% to 30.0% of vinyl resin or polyester resin or PVC resin or amino resin in 70% to 90% of ethylene glycol ether or terpineol or cyclohexyl by mass percentage One or several solvents in the ketone, and then heated at a constant temperature of 70-90°C until completely dissolved, and filtered to obtain an organic carrier;
[0021] Step 2): Prepare a mixed solution of two conductive phases of nickel powder and silver powder
[0022] Adding 60% to 80% of superfine nickel powder (60 to 200nm in particle size) by mass percentage into 20.0% to 40.0% of the above-mentioned organic carrier, and stirring evenly to prepare a superfine nickel powder mixed solution;
[0023] Add 5% to 30.0% of spherical silver powder (with a particle size of 0.4 to 1.2um) and 50.0% to...
Embodiment 1
[0030] Firstly, under constant temperature condition of 70° C., 5 grams of vinyl acetate resin was dissolved in 40 grams of ethylene glycol ether and 5 grams of terpineol, and the organic carrier was obtained by filtration.
[0031] Then add 24 grams of nickel powder (60-100nm) to 16 grams of the above-mentioned organic vehicle; 5 grams of spherical silver powder (0.4-1.0um) and 30 grams of flake silver powder (1.4-5.0um) are added to 15 grams of the above-mentioned organic vehicle 0.1 g of polyethylene wax dispersant was added respectively, and mixed uniformly to obtain a mixed solution of the above two conductive phases.
[0032] Finally, the nickel powder mixed solution of 5 grams and the silver powder mixed solution of 35 grams are combined and mixed, and 1.5 grams of γ-aminopropyltriethoxysilane thickener and 0.1 gram of polyethylene wax dispersant are added in the combined mixed solution , mixed evenly in a planetary mixer, after passing through a three-roll mill, adding...
Embodiment 2
[0034] First, 10 grams of vinyl acetate resin and 5 grams of polyester resin were dissolved in 20 grams of ethylene glycol ether and 15 grams of terpineol at a constant temperature of 75° C., and filtered to obtain an organic carrier.
[0035] Then add 32 grams of nickel powder (60-150nm) to 8 grams of the above-mentioned organic vehicle; 15 grams of spherical silver powder (0.6-1.2um) and 25 grams of flake silver powder (2.4-9.0um) are added to 10 grams of the above-mentioned organic vehicle 0.4 g of microcrystalline paraffin dispersant was added respectively, and mixed uniformly to obtain a mixed solution of the above two conductive phases.
[0036] Finally, 25 grams of nickel powder mixed solution and 20 grams of silver powder mixed solution are combined and mixed, and 1.0 gram of vinyl tris (beta-methoxyethoxy) silane thickener and 0.4 gram of micro Crystal paraffin wax dispersant, mixed evenly in a planetary mixer, after passing through a three-roll mill, adding 3.6 grams...
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