Method for preparing viscose fibers through ultrasonic depolymerization of bamboo and bombax composite pulp
A technology of composite pulp and viscose fiber, applied in the field of viscose fiber manufacturing, can solve problems such as unstable product quality, large area of reaction kettle, and uneven reduction of polymerization, so as to reduce process control points and prevent uneven reaction Uniform, avoiding the effect of reducing poly dead angle
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Embodiment 1
[0046] The specific process steps are as follows:
[0047]1. Put bamboo pulp, wood pulp and cotton pulp with an average degree of polymerization greater than 1000 on the pulp feeder, set a certain feeding speed (25kg / min), then add a concentration of 85g / l, and the temperature is 60℃~ 90 ℃ lye, lye flow rate is 10m 3 / h~20m 3 , and then through stirring, the pulp is broken and fully mixed with lye to prepare a solid and liquid mixture, which is called composite pulp porridge, and this process is called impregnation in technology.
[0048] Function: Make bamboo pulp, wood pulp and cotton pulp raw materials into a solid and liquid mixture, dissolve β-cellulose at the same time, increase the content of α-fiber, and produce alkali cellulose.
[0049] Control parameters: lye temperature: 75±15°C lye concentration: 85g / l
[0050] Compound pulp porridge concentration: 3.5±2% (mass percentage) Dipping time: 30±20min
[0051] Alternatively, the above cotton pulp, bamboo p...
Embodiment 2
[0063] The specific process steps are as follows:
[0064] 1. Put bamboo pulp, wood pulp, and cotton pulp with an average degree of polymerization greater than 800 on the pulp feeder, set a certain feeding speed (25kg / min), then add a concentration of 80g / l, and the temperature is 60°C~ 90 ℃ lye, lye flow rate is 10m 3 / h~20m 3 , whose purpose is to accelerate the dissolution of lignin and impurities in bamboo pulp and wood pulp. Then, through stirring, the pulp is crushed and fully mixed with lye to prepare a mixture of solid and liquid, which is called composite pulp porridge, and this process is called impregnation in technology.
[0065] Function: Make bamboo pulp, wood pulp, and cotton pulp raw materials into a solid and liquid mixture. The process is called impregnation. At the same time, it dissolves β-cellulose, increases the content of α-fiber, and produces alkali cellulose.
[0066] Control parameters: lye temperature: 75±15°C lye concentration: 80g / l
[0067] ...
Embodiment 3
[0080] The specific process steps are as follows:
[0081] 1. Put bamboo pulp, wood pulp, and cotton pulp with an average degree of polymerization greater than 1200 on the pulp feeder, set a certain feeding speed (25kg / min), then add a concentration of 100g / l, and the temperature is 60℃~ 90 ℃ lye, lye flow rate is 10m 3 / h~20m 3 , while adding lye, add auxiliary agent: methyl isopropyl ketone (MIBK)-ethanol mixed solvent, wherein MIBK: ethanol=80:50, its purpose is to accelerate the dissolution of lignin and impurities in bamboo pulp and wood pulp . Then, through stirring, the pulp is crushed and fully mixed with lye to prepare a mixture of solid and liquid, which is called composite pulp porridge, and this process is called impregnation in technology.
[0082] Function: Make bamboo pulp, wood pulp, and cotton pulp raw materials into a solid and liquid mixture. The process is called impregnation. At the same time, it dissolves β-cellulose, increases the content of α-fiber, ...
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