Method for preparing viscose fibers through ultrasonic depolymerization of bamboo and bombax composite pulp

A technology of composite pulp and viscose fiber, applied in the field of viscose fiber manufacturing, can solve problems such as unstable product quality, large area of ​​reaction kettle, and uneven reduction of polymerization, so as to reduce process control points and prevent uneven reaction Uniform, avoiding the effect of reducing poly dead angle

Inactive Publication Date: 2012-07-04
YIBIN HIEST FIBER +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] 1. Uneven depolymerization: Due to the large volume of the reactor and many dead spots in the stirring, the stirring is uneven; and the addition of oxygen cannot evenly penetrate into the porridge to participate in the reaction, which eventually leads to uneven depolymerization;
[0008] 2. The reaction kettle occupies a large area, and requires compressed air and high temperature environment, which makes the whole viscose fiber production process become huge, time-consuming, with many equipments and large workshop area, which is not convenient for production management;
[0009] 3. The work of the reactor requires compressed air and steam, which consumes a lot of energy
[0010] 4. The reaction in the reaction kettle is under high temperature, aerobic and stirring conditions. There are many process control points and difficult control, resulting in unstable product quality.

Method used

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  • Method for preparing viscose fibers through ultrasonic depolymerization of bamboo and bombax composite pulp
  • Method for preparing viscose fibers through ultrasonic depolymerization of bamboo and bombax composite pulp
  • Method for preparing viscose fibers through ultrasonic depolymerization of bamboo and bombax composite pulp

Examples

Experimental program
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Effect test

Embodiment 1

[0046] The specific process steps are as follows:

[0047]1. Put bamboo pulp, wood pulp and cotton pulp with an average degree of polymerization greater than 1000 on the pulp feeder, set a certain feeding speed (25kg / min), then add a concentration of 85g / l, and the temperature is 60℃~ 90 ℃ lye, lye flow rate is 10m 3 / h~20m 3 , and then through stirring, the pulp is broken and fully mixed with lye to prepare a solid and liquid mixture, which is called composite pulp porridge, and this process is called impregnation in technology.

[0048] Function: Make bamboo pulp, wood pulp and cotton pulp raw materials into a solid and liquid mixture, dissolve β-cellulose at the same time, increase the content of α-fiber, and produce alkali cellulose.

[0049] Control parameters: lye temperature: 75±15°C lye concentration: 85g / l

[0050] Compound pulp porridge concentration: 3.5±2% (mass percentage) Dipping time: 30±20min

[0051] Alternatively, the above cotton pulp, bamboo p...

Embodiment 2

[0063] The specific process steps are as follows:

[0064] 1. Put bamboo pulp, wood pulp, and cotton pulp with an average degree of polymerization greater than 800 on the pulp feeder, set a certain feeding speed (25kg / min), then add a concentration of 80g / l, and the temperature is 60°C~ 90 ℃ lye, lye flow rate is 10m 3 / h~20m 3 , whose purpose is to accelerate the dissolution of lignin and impurities in bamboo pulp and wood pulp. Then, through stirring, the pulp is crushed and fully mixed with lye to prepare a mixture of solid and liquid, which is called composite pulp porridge, and this process is called impregnation in technology.

[0065] Function: Make bamboo pulp, wood pulp, and cotton pulp raw materials into a solid and liquid mixture. The process is called impregnation. At the same time, it dissolves β-cellulose, increases the content of α-fiber, and produces alkali cellulose.

[0066] Control parameters: lye temperature: 75±15°C lye concentration: 80g / l

[0067] ...

Embodiment 3

[0080] The specific process steps are as follows:

[0081] 1. Put bamboo pulp, wood pulp, and cotton pulp with an average degree of polymerization greater than 1200 on the pulp feeder, set a certain feeding speed (25kg / min), then add a concentration of 100g / l, and the temperature is 60℃~ 90 ℃ lye, lye flow rate is 10m 3 / h~20m 3 , while adding lye, add auxiliary agent: methyl isopropyl ketone (MIBK)-ethanol mixed solvent, wherein MIBK: ethanol=80:50, its purpose is to accelerate the dissolution of lignin and impurities in bamboo pulp and wood pulp . Then, through stirring, the pulp is crushed and fully mixed with lye to prepare a mixture of solid and liquid, which is called composite pulp porridge, and this process is called impregnation in technology.

[0082] Function: Make bamboo pulp, wood pulp, and cotton pulp raw materials into a solid and liquid mixture. The process is called impregnation. At the same time, it dissolves β-cellulose, increases the content of α-fiber, ...

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Abstract

The invention provides a method for preparing viscose fibers through ultrasonic depolymerization of bamboo and bombax composite pulp, which is a method for producing the viscose fibers from bamboo and bombax mixed slurry through depolymerization in an ultrasonic depolymerization tube. In the method, a traditional reaction kettle is replaced by the ultrasonic depolymerization tube, and the method comprises the following steps of: performing alkali steeping on the bamboo and bombax pulp to obtain slurry; depolymerizing the slurry under the action of an ultrasonoscope; and pressing to obtain alkaline fibers, and finally preparing the viscose fibers from the alkaline fibers. The method overcomes the defects in the prior art, the depolymerization is more uniform, the energy consumption is low,a few pieces of equipment are used, the occupied space is small and the product quality is stable. Moreover, the ultrasonic polymer depolymerization is applied to production of the viscose fibers forthe first time, and a depolymerization method for the production of the viscose fibers through depolymerization is increased.

Description

technical field [0001] The invention belongs to the field of viscose fiber production, and relates to a method for producing viscose fiber with bamboo kapok composite pulp, specifically a method for producing fiber viscose fiber with bamboo kapok composite pulp by applying an ultrasonic depolymerization method. technical background [0002] The depolymerization of cellulose (reducing the degree of polymerization) is an indispensable process step in the production of viscose. Only by reducing the depolymerization of plant cellulose to a certain extent can the production requirements of subsequent viscose fibers be met, and the uniformity of depolymerization in it And the degree of depolymerization is the key to depolymerization of cellulose. [0003] The reduction methods of cellulose for preparing viscose include: aerobic reduction and alkali reduction. In actual application, aerobic polymerization is the main method, while alkaline polymerization requires relatively high t...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F2/06C08B1/08C08B9/00
Inventor 冯涛邓传东李蓉玲梁建军唐孝兵田启兵严青平胡小东施洋范怀熙
Owner YIBIN HIEST FIBER
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