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Chinese medicine composition for regulating qi, widening chest and relieving pain as well as detection method thereof

A composition and technology of traditional Chinese medicine, applied in traditional Chinese medicine composition for pain relief, traditional Chinese medicine composition and quality control thereof, in the field of regulating qi and widening chest, can solve problems such as large side effects, difficult to achieve fundamental treatment, etc., achieve rapid results, effective quality control, Identify the specificity of the good effect

Active Publication Date: 2011-06-22
BEIJING ASIA EAST BIO PHARMA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Nitrate drugs, calcium ion antagonists, and β-receptor blockers are commonly used in clinical treatment and control of angina pectoris, but these drugs have relatively large side effects and are difficult to achieve the purpose of fundamental treatment

Method used

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  • Chinese medicine composition for regulating qi, widening chest and relieving pain as well as detection method thereof
  • Chinese medicine composition for regulating qi, widening chest and relieving pain as well as detection method thereof
  • Chinese medicine composition for regulating qi, widening chest and relieving pain as well as detection method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0091]Preparation of the test solution: Take 1 g of this product, put it in a mortar, add 5-10 ml of ether, grind, filter, put the filtrate in an evaporating dish, evaporate the ether, cover the watch glass, heat it on a water bath, and collect the sublimation , add ethanol 1ml to dissolve, as the test solution.

[0092] Preparation of reference substance solution: take borneol reference substance, add ethanol to make a solution containing 1mg per 1ml, as the reference substance solution.

[0093] Preparation of negative reference substance solution: prepare a negative reference substance lacking borneol according to the preparation method of the test sample, and then prepare a negative reference substance solution according to the preparation method of the test sample solution.

[0094] A. The choice of developer

[0095] According to the thin-layer chromatography (Chinese Pharmacopoeia, 2005 edition, an appendix VIB) test, absorb 3 μl of the above-mentioned test solution an...

Embodiment 1

[0143] Take the following parts by weight (g) bulk drug:

[0144] Styrax 65g, borneol 125g, frankincense (made) 95g, agarwood 165g, woody 235g

[0145] The above five flavors, except storax and borneol, add 10 times the amount of water to extract the volatile oil of the other three flavors such as frankincense, and extract the dregs with 4 times the amount of 80% ethanol under reflux for two times, each time for 2 hours, filter, and recycle the ethanol from the filtrate to nothing Alcoholic taste, concentrated under reduced pressure to a thick paste with a relative density of 1.25-1.30, dried, crushed into fine powder, added styrax, borneol and 220g of polyethylene glycol 6000 base, heated until dissolved, then added the above-mentioned frankincense and other volatile oils, and mixed well , made into 450g dropping pills, to get final product.

Embodiment 2

[0147] Take the following parts by weight (g) bulk drug:

[0148] Artificial musk 35g, borneol 125g, frankincense (made) 95g, sandalwood 165g, inulin 235g

[0149] The above five flavors, except artificial musk and borneol, add 10 times the amount of water to extract the volatile oils of the other three flavors such as frankincense, and extract the dregs with 4 times the amount of 80% ethanol by heating and refluxing twice, each time for 2 hours, filter, and the filtrate recovers ethanol to No alcohol smell, concentrated under reduced pressure to a thick paste with a relative density of 1.25-1.30, dried, crushed into fine powder, added styrax, borneol and 220g of polyethylene glycol 6000 base, heated until dissolved, then added the above-mentioned frankincense and other volatile oils, mixed Evenly, make 430g dropping pills, to get final product.

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Abstract

The invention discloses a Chinese medicine composite for regulating qi, widening chest and relieving pain and for treating stenocardia and abdominal distending pain as well as a quality control method thereof. The Chinese medicine composite is a pill made from raw medicinal materials of storax, borneol, frankincense, agilawood and radix aucklandiae. The quality control method comprises the steps of thin-layer identification of the frankincense and the borneol and content determination of the borneol and can more comprehensively control the quality of drugs in qualitative and quantitative aspects. Pharmacodynamics tests show that the Chinese medicine composite provided by the invention has better treatment effect on treating the stenocardia and the abdominal distending pain.

Description

[0001] The present invention is a divisional application, the original application number is 200810102915.8, the original application date is March 28, 2008, and the original application name is a traditional Chinese medicine composition for regulating qi, broadening the chest and relieving pain and its quality control method. technical field [0002] The invention relates to a traditional Chinese medicine composition and a quality control method thereof, in particular to a traditional Chinese medicine composition for regulating qi, broadening the chest and relieving pain and a quality control method of the traditional Chinese medicine composition, belonging to the technical field of traditional Chinese medicine. Background technique [0003] Angina pectoris is a clinical syndrome caused by coronary insufficiency, myocardial acute, temporary ischemia and hypoxia. It is characterized by paroxysmal chest squeezing pain, which may be accompanied by other symptoms. The pain is ma...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/835A61K36/324A61K36/54G01N30/02G01N30/38G01N30/90A61P9/10A61K31/045A61K31/122
Inventor 付立家付建家
Owner BEIJING ASIA EAST BIO PHARMA CO LTD
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