Deodorization polyamide fiber and preparation method thereof

A deodorizing polyamide and polyamide fiber technology, applied in the field of polyamide fiber, can solve the problems of uneven dispersion, human body irritation, easy washing and loss, etc., and achieve the effect of reducing material consumption, simplifying production process and reducing production cost

Active Publication Date: 2013-11-06
FUJIAN JINJIANG TECH
View PDF4 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Since these functional components are only in the form of free mixing and have not formed bonds with fiber molecules, a series of problems such as uneven dispersion, poor adhesion, and easy elution and loss are caused; secondly, functional components are mixed into the spinning solution , due to failure to form a whole with the fiber, it will inevitably cause defects, and may cause technical problems such as broken filaments during the spinning process; on the other hand, the functional agent may also have certain irritation or toxicity. While being lost during use, it may contact the human body and cause irritation and toxicity to the human body

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0035] A method for preparing deodorant polyamide fiber, which is prepared from the following raw materials in weight percentage: 100-300 parts of polyamide fiber, 0.5-2 parts of 2-bromo-2-nitro-1,3-propanediol, solvent 200-500 parts, 0.05-0.2 parts of dehydrating agent and a small amount of catalyst.

[0036] (1) Put the raw materials into the reactor according to the ratio of 0.5-2 parts of 2-bromo-2-nitro-1,3-propanediol and 200-500 parts of solvent, and dissolve at 40°C-80°C;

[0037] (2) Add 0.05-0.2 parts of dehydrating agent and 0.1-0.2 parts of catalyst to the solution obtained in step (1), mix well, then add 100-300 parts of polyamide fibers, adjust the temperature to reflux temperature, and dry in ultrasonic or Reflux reaction under inert gas stirring for 1~10h;

[0038] (3) After the reaction is completed, take out the polyamide fiber and centrifuge to recover the solution;

[0039] (4) The polyamide fibers from which the solution has been removed by centrifugatio...

Embodiment 1

[0041] (1) Put the raw materials into the reactor according to the ratio of 1 part of 2-bromo-2-nitro-1,3-propanediol and 200 parts of acetone, and dissolve at 50°C;

[0042] (2) Add 0.2 parts of phosphorus pentoxide and 0.1 parts of hydrochloric acid to the solution obtained in step (1), mix well, then add 100 parts of nylon-6 fiber, adjust the temperature to the reflux temperature, and reflux for 1 hour under ultrasonic stirring ;

[0043] (3) After the reaction is completed, take out the nylon-6 fiber and centrifuge to recover the solution;

[0044] (4) The nylon-6 fibers from which the solution has been removed by centrifugation are washed and then dried to obtain the deodorized nylon-6 fibers.

Embodiment 2

[0046] (1) Put the raw materials into the reactor according to the ratio of 5 parts of 2-bromo-2-nitro-1,3-propanediol and 500 parts of ethanol, and dissolve at 70°C;

[0047] (2) Add 10 parts of anhydrous sodium sulfate and 0.05 parts of sulfuric acid to the solution obtained in step (1), mix well, then add 250 parts of nylon-6,6 fiber, adjust the temperature to reflux temperature, and stir under dry nitrogen Reflux reaction for 5h;

[0048] (3) After the reaction is completed, take out the nylon-6,6 fiber, and centrifuge to recover the solution;

[0049] (4) The nylon-6,6 fibers from which the solution has been removed by centrifugation are washed and then dried to obtain the deodorized nylon-6,6 fibers.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention discloses a deodorization polyamide fiber and a preparation method thereof. The deodorization polyamide fiber comprises the following raw material components in part by weight: 100 to 300 parts of polyamide fiber, 0.5 to 2 parts of 2-bromine-2-nitro-1,3-propylene glycol, 200 to 500 parts of solvent, 0.05 to 0.2 part of dehydration agent and 0.1 to 0.2 part of catalyst. The preparation method comprises the following steps of: reacting the 2-bromine-2-nitro-1,3-propylene glycol which has a deodorization function with the polyamide fiber to ensure that hydroxyl in 2-bromine-2-nitro-1,3-propylene molecules and carboxyl in polyamide molecules are subjected to condensation reaction, and thus obtaining the polyamide fiber with the deodorization function. By bonding the 2-bromine-2-nitro-1,3-propylene glycol with polyamide macromolecules, the improvement on the stability of the deodorization polyamide fiber is facilitated, the deodorization polyamide fiber difficultly runs away in the using process, and the laundering durability of the deodorization polyamide fiber is improved; and simultaneously, the safety of the deodorization polyamide fiber can be improved, and the deodorization polyamide fiber has obvious economic and social benefits.

Description

technical field [0001] The invention relates to the technical field of polyamide fibers, in particular to a deodorizing polyamide fiber and a preparation method thereof. Background technique [0002] There are various bacteria and molds in the human living environment, and the reproduction of these microorganisms is particularly active in high-temperature and humid environments. When bacteria and molds multiply on clothing, the fibers are susceptible to molecular chain degradation and discoloration due to the action of their acidic or basic metabolites, and generate volatile odorous substances, which can also easily cause some skin diseases in the human body. Therefore, in order to meet people's high requirements for the hygienic function of textiles, antibacterial, deodorant and deodorizing processing of fiber products is very necessary. [0003] There are tens of thousands of odorous substances, among which ammonia, methyl mercaptan, trimethylamine and hydrogen sulfide ar...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Patents(China)
IPC IPC(8): D06M13/392D06M11/55D06M11/70D06M11/155D06M11/69D06M101/34
Inventor 甘纯玑吴道斌
Owner FUJIAN JINJIANG TECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap