Quality detection method for Chinese herbal compound preparation for replenishing Qi and nourishing Yin
A compound preparation and detection method technology, applied in the field of quality inspection of traditional Chinese medicine compound preparations, can solve problems such as few quality control indicators, inability to effectively control the quality of Xinnaoshu preparations, affecting product production quality control and drug safety, and achieve specificity Good, production quality control and medication safety assurance, good reproducible effect
Active Publication Date: 2014-04-23
RONGCHANG PHARM ZIBO CO LTD
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Problems solved by technology
But existing preparation standard is backward, and quality control index is few, only has the TLC identification item of ginseng reference substance, and the quality detection method of prior art can't effectively control the quality of Xinnaoshu preparation, thereby will influence the production quality control of product and medication safety
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Embodiment 1
[0072] Prescription: Ginseng 70g, Ophiopogon japonicus 137.5g, Schisandra 92.5g, Codonopsis 92.5g, Astragalus 47.5g;
[0073] Preparation method: the above five flavors and ginseng are extracted four times with 85% ethanol under reflux, each time for 3 hours, the extracts are combined, filtered, and the filtrate is recovered from ethanol and concentrated into a thick paste; Ophiopogon japonicus, dangshen, and astragalus are decocted three times, and the first 3 hours for the first time, 2 hours for the second time, 1 hour for the third time, combine the decoction, filter, concentrate the filtrate to an appropriate amount, add ethanol to make the alcohol content reach 70%, stir well, leave it for more than 12 hours, and take the supernatant Recover ethanol and condense into a thick paste, combine the above thick pastes, add water and activated carbon, the activated carbon accounts for 0.3% of the total mass of the thick paste; boil, refrigerate for more than 12 hours, filter, an...
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Abstract
The invention relates to a quality detection method for a Chinese herbal compound preparation, in particular to the quality detection method for the Chinese herbal compound preparation for replenishing Qi and nourishing Yin and a preparation method thereof. The quality detection method provides an identification detection method of ginseng, astragalus mongholicus and schisandra chinensis in the Chinese herbal compound preparation for replenishing Qi and nourishing Yin and a chromatographic detection method for content of ginsenoside Rg1. The quality detection method is capable of effectively controlling quality of the cardio-cerebral easiness preparation, good in specificity and reproducibility and strong in stability, and accordingly ensures production quality control of products and drug safety.
Description
technical field [0001] The invention relates to a quality detection method of a Chinese medicine compound preparation, in particular to a quality detection method of a Chinese medicine compound preparation for invigorating qi and nourishing yin. Background technique [0002] Xinnaoshu oral preparation is a compound preparation of traditional Chinese medicine that has been marketed, which has the effect of nourishing qi and nourishing yin. Clinically, it is mainly used for dizziness, insomnia, forgetfulness, palpitations, shortness of breath, fatigue, spontaneous sweating and night sweats, and impatient fatigue caused by deficiency of both qi and yin. But existing preparation standard is backward, and quality control index is few, only has the TLC identification item of ginseng reference substance, and the quality detection method of prior art can't effectively control the quality of Xinnaoshu preparation, thereby will influence the production quality control of product and ...
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IPC IPC(8): G01N30/90G01N30/02
Inventor 翟勇郭桂秋王荔强王丽庆郗光健李雪梅时延利
Owner RONGCHANG PHARM ZIBO CO LTD