Cooling process of czochralski single-crystal method
A Czochralski, single crystal technology, applied in the field of solar photovoltaic, can solve the problems of short residence time, high cooling gas cost, general cooling effect, etc., and achieve the effect of reducing usage and production cost.
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Embodiment 1
[0009] A cooling process of the Czochralski single crystal method. After the cooling stage is carried out for 0.8 hours, the temperature in the furnace drops to 1220 ° C and the pressure is 30 Pa. Stop feeding argon into the furnace and turn off the vacuum pump to form a In the pressure-holding state, the pressure is 50 Pa, and it is maintained for 4.2 hours until the whole Czochralski method single crystal preparation process ends.
Embodiment 2
[0011] A cooling process of the Czochralski single crystal method. After the cooling stage is carried out for 1.0h, the temperature in the furnace drops to 1250°C and the pressure is 32Pa. Stop feeding argon into the furnace and turn off the vacuum pump to form a In the pressure-holding state, the pressure is 53 Pa, and it is maintained for 4.5 hours until the whole Czochralski method single crystal preparation process ends.
Embodiment 3
[0013] A cooling process of the Czochralski single crystal method. After the cooling stage is carried out for 1.2 hours, the temperature in the furnace drops to 1280 ° C and the pressure is 34 Pa. Stop feeding argon into the furnace and turn off the vacuum pump to form a In the pressure-holding state, the pressure is 56 Pa, and it is maintained for 4.8 hours until the whole Czochralski method single crystal preparation process ends.
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