High viscosity polyvinyl chloride paste resin PE1311 and preparation method thereof

A polyvinyl chloride paste and high-viscosity technology, applied in the field of vinyl chloride polymerization in the chlor-alkali chemical industry, can solve the problems of reduced product aging performance, unstable reduction system, and unstable polymerization reaction, and achieve improved aging performance, easy operation, and reduction The effect of system stability

Inactive Publication Date: 2013-04-24
ANHUI TIANCHEN CHEM
View PDF0 Cites 10 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented technology describes making highly concentrated or clear liquid plastics with specific properties such as low stickiness (low gloss) at room temperatures). These liquids are made from vinylchloride monomer solution which contains iron salts like Ferrum Sulfate for better stability during storage over time without losing their desired qualities.

Problems solved by technology

This patented technology describes different methods for producing plastic materials called polystyrene (PS) particles or vinylchloride (VCM). These techniques involve reactants containing certain chemical compounds together through heat treatment at specific temperatures. By controllably varying these parameters during processing, desired properties such as particle sizes are achieved without affecting stability over time. However, this results in decreased production efficiency due to increased costs associated with post-processing operations like cleanings and solvent extraction processes. To solve this problem, we have developed an improved version of the original formulation described earlier on how to achieve better quality products from PS particles.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • High viscosity polyvinyl chloride paste resin PE1311 and preparation method thereof
  • High viscosity polyvinyl chloride paste resin PE1311 and preparation method thereof
  • High viscosity polyvinyl chloride paste resin PE1311 and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Example 1 Preparation of PE1311-01 resin, the formula is shown in Table 1, and the preparation method is as follows:

[0029] (1) Add 350kg of ion-free water into the polymerization kettle, and add 1kg of sodium laurate, 2kg of ferrous sulfate and 4kg of white block under stirring;

[0030] (2) Then vacuum deoxidize the polymerization kettle, add 400kg of vinyl chloride monomer, and raise the temperature of the polymerization kettle to 60°C;

[0031] (3) Dissolve 2kg of sodium persulfate and 15kg of sodium dodecylbenzenesulfonate completely in deionized water;

[0032] (4) Continuously add the sodium persulfate solution and sodium dodecylbenzenesulfonate solution dissolved in water into the polymerization kettle, keep stirring, and the polymerization reaction occurs. Control the temperature of the reaction system at 60°C. When the polymerization kettle After the pressure reached 10MPa, the pressure of the polymerization tank began to drop, and when the pressure dropped...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention provides a high viscosity polyvinyl chloride paste resin PE1311 and a preparation method thereof. The high viscosity polyvinyl chloride paste resin PE1311 is prepared from raw materials comprising, by weight part ratio, 100-600 parts of vinyl chloride monomer, 100-600 parts of water, 1-10 parts of sodium persulfate, 1-10 parts of ferrous sulfate, 1-5 parts of sodium laurate, 10-50 parts of sodium dodecyl benzene sulfonate and 1-5 parts of sodium formaldehyde sulfoxylate. The preparation method includes: adopting an emulsion polymerization method for producing, adding monomers and addition agents into a polymerizing pot according to the weight part ratio, exhausting oxygen, aerating nitrogen, raising temperature to 50-60 DEG C under a stirring state, maintaining the temperature for a polymerization reaction, and finishing the reaction when pressure reaches 10MPa. The preparation method is simple in technology and easy to operate, and furthermore the produced product has the advantages of being high in paste viscosity, high in foaming ratio and good in rheological property.

Description

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Owner ANHUI TIANCHEN CHEM
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products