Thermal storage fiber and preparation method thereof
A heat storage fiber and heat storage technology, which is applied in the fields of fiber chemical characteristics, wet spinning, rayon manufacturing, etc., can solve the problems of unsustainable heat storage effect of fibers, poor chemical stability of zirconium carbide, and unsatisfactory heat preservation effect, etc., to achieve Reduce the cost of dyeing treatment, save the dyeing process, and improve the effect of microcirculation
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Embodiment 1
[0023] The preparation method of a kind of heat storage fiber of embodiment 1, mix 92~94wt% acrylonitrile, 6~8wt% vinyl acetate two monomers, and adjust the concentration after mixing to 30~40wt%, in 58~ Continuous suspension copolymerization in water at 62°C and pH 2.5 to 3.5; the reacted copolymer powder is terminated by chelation reaction, the unreacted monomer is removed by a stripper, and then the salt and water are removed by washing and filtering. After granulation and molding, the copolymer powder formed by acrylonitrile and vinyl acetate is obtained by drying; the copolymer powder and dimethylacetamide are mixed and dissolved at a mass ratio of 1:3, and the temperature is raised to 80-90 ° C to make the copolymer powder Dissolve the powder in dimethylacetamide completely, and then lower the temperature to 70-80°C to filter the obtained spinning stock solution, adjust the temperature and pressure, and filter at 0.7-0.9MPa pressure and 92-97°C. Spinning, during the spin...
Embodiment 2
[0024] The preparation method of a kind of heat storage fiber of embodiment 2, mix 92~94wt% acrylonitrile, 6~8wt% vinyl acetate two monomers, and adjust the concentration after mixing to 30~40wt%, at 58~ Continuous suspension copolymerization in water at 62°C and pH 2.5 to 3.5; the reacted copolymer powder is terminated by chelation reaction, the unreacted monomer is removed by a stripper, and then the salt and water are removed by washing and filtering. After granulation and molding, the copolymer powder formed by acrylonitrile and vinyl acetate is obtained by drying; the copolymer powder and dimethylacetamide are mixed and dissolved at a mass ratio of 1:3, and the temperature is raised to 80-90 ° C to make the copolymer powder Dissolve the powder in dimethylacetamide completely, and then lower the temperature to 70-80°C to filter the obtained spinning stock solution, adjust the temperature and pressure, and filter at 0.7-0.9MPa pressure and 92-97°C. Spinning, during the spin...
Embodiment 3
[0025] The preparation method of a kind of heat storage fiber of embodiment 3, mix 92~94wt% acrylonitrile, 6~8wt% vinyl acetate two monomers, and adjust the concentration after mixing to 30~40wt%, in 58~ Continuous suspension copolymerization in water at 62°C and pH 2.5 to 3.5; the reacted copolymer powder is terminated by chelation reaction, the unreacted monomer is removed by a stripper, and then the salt and water are removed by washing and filtering. After granulation and molding, the copolymer powder formed by acrylonitrile and vinyl acetate is obtained by drying; the copolymer powder and dimethylacetamide are mixed and dissolved at a mass ratio of 1:3, and the temperature is raised to 80-90 ° C to make the copolymer powder Dissolve the powder in dimethylacetamide completely, and then lower the temperature to 70-80°C to filter the obtained spinning stock solution, adjust the temperature and pressure, and filter at 0.7-0.9MPa pressure and 92-97°C. Spinning, during the spin...
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