Fluorine-free water-proofing agent and preparation method thereof as well as textile
A fluorine-free waterproofing agent and hydrophilic agent technology, applied in the field of textile auxiliaries, can solve the problems of waterproofing and washing resistance of waterproofing agents, and achieve good binding force, waterproof performance and washing resistance.
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Embodiment 1
[0041] Take 50.64 grams of hexamethylene diisocyanate, 66.69 grams of isophorone diisocyanate, 26.84 grams of trimethylolpropane, 65 grams of polyethylene glycol phthalate polyol, 8.75 grams of polyoxyethylene ether Add polyhydric alcohol, 5.96 grams of N-methyldiethanolamine, and 24.03 grams of 3,5-dimethylpyrazole into the reaction kettle, and react at 70-80° C. to obtain polyurethane.
[0042] Add 6 grams of acetic acid, 240 grams of acetone, 248 grams of paraffin wax with a melting range of 63 to 68 °C, and 50 grams of Ethoqual C / 25 (ethoxylated quaternary ammonium salt) into polyurethane, and stir well; add 1350 grams of water to emulsify at high speed; then reduce Remove acetone by pressure distillation, add water to adjust the solid content to 30%, and obtain a fluorine-free waterproofing agent.
[0043] other embodiments
[0044] Each component in other examples is different from Example 1, and the preparation process is the same as Example 1. Below, the components of...
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