Reactive ionic liquid and ion-immobilized metal oxide particle, ion-immobilized elastomer, and converter using same
A technology of reactive ions and oxide particles, applied in the direction of titanium oxide/hydroxide, compounds of elements of group 4/14 of the periodic table, compounds of elements of group 5/15 of the periodic table, etc., can solve the problem of high resistance, etc. problem, to achieve the effect of inhibiting insulation breakdown
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Embodiment 1
[0109]
[0110] In 5.0 g of a solution of 1-butyl-3-methylimidazolium bicarbonate (solvent: methanol / water = 3:2 mixture, concentration: 50% by mass, 0.0125 mol), dropwise on an ice bath, etc. Moles of acrylic acid monomer (0.0125 mol). At this time, bubble generation was confirmed. After 30 minutes, return to room temperature and stir for 6 hours. After the solvent was distilled off under reduced pressure, methanol (super-dehydrated) (Wako Pure Chemical Industries, Ltd.) was added, and the solvent was distilled off again under reduced pressure. Through the above operations, the ionic liquid monomer was obtained by the acid ester method. Next, 2.10 g (10.0 mmol) of the obtained ionic liquid monomer and 1.87 mL (10.1 mmol) of 3-mercaptopropyltrimethoxysilane were dissolved in 20 mL of methanol (super-dehydrated). As a catalyst, 10 mol% of diisopropylamine was added to 3-mercaptopropyltrimethoxysilane, stirred at room temperature for 20 hours, and evaporated to obtain a rea...
Embodiment 2
[0113]
[0114] In the ester method, 9.75 g of a solution of 1-ethyl-1-methylmorpholinium methyl carbonate (solvent: methanol / water = 2:3 mixed solution, concentration 50% by mass, 0.0238 mol) and Equimolar 2-acrylamide-2-methylpropanesulfonic acid (0.0238mol), in addition, with the synthetic operation of reactive ionic liquid (13), obtain the reactive ionic liquid ( 16).
[0115]
Embodiment 3
[0117]
[0118] In the ester method, 10.11 g of a solution of tributylmethylammonium methyl carbonate (solvent: methanol / water = 2:3 mixture, concentration of 50% by mass, 0.0244 mol) and equimolar 2-acrylamide- Except for 2-methylpropanesulfonic acid (0.0244 mol), a reactive ionic liquid (17) represented by the following structural formula was obtained in the same manner as the synthesis of the reactive ionic liquid (13).
[0119]
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