Multi-mode extraction of soluble matter in solids and solvent distillation recovery storage method and device
A distillation recovery, multi-mode technology, applied in solid solvent extraction, distillation in boilers/distillates, etc., can solve the problems of inability to store solvents, cumbersome experimental operations, and inability to completely block the discharge of liquids, so as to speed up the extraction speed Effect
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Embodiment 1
[0036] Embodiment 1: as figure 1 , figure 2 , image 3 , Figure 4 , Figure 5 , Figure 6 , Figure 7 , Figure 8 , Figure 9 As shown, the multi-mode extraction and solvent distillation recovery storage device for solubles in solids consists of extraction chamber 1, communication pipe 2, air guide pipe 3, bottom liquid return pipe 4, high liquid level siphon return pipe 5 and the first control valve 6 and the second control valve 7 constitute;
[0037] The central part 8 of the bottom of the extraction chamber 1 is convex, and the upper mouth 9 of the extraction chamber 1 is in the shape of an inner grinding mouth. The maximum volume of the liquid in the extraction chamber 1 is greater than the volume of the solvent used during extraction; the connecting pipe 2 is connected to the lower end of the extraction chamber 1, The lower end of the connecting pipe 2 is an external grinding port 10; the lower end of the air guide pipe 3 communicates with the connecting pipe 2...
Embodiment 2
[0038] Embodiment 2: Multi-mode extraction of soluble matter in solids and solvent distillation recovery storage device, such as Figure 10 , Figure 11 , Figure 12 , Figure 13 , Figure 14 , Figure 15 Shown, structure is identical with embodiment 1, difference is:
[0039] The lower end of the bottom liquid return pipe 4 communicates with the third radial inlet 18 of the third control valve 17; one end of the high liquid level siphon return pipe 5 communicates with the bottom liquid return pipe 4, and the high liquid level siphon return pipe 5 The other end communicates with the fourth radial inlet 19 of the third control valve 17; the third control valve 17 is a three-way valve with the third radial inlet 18, the fourth radial inlet 19 and the third axial outlet 20, The included angle between the third radial inlet 18 and the fourth radial inlet 19 is less than 180 degrees, and the third axial outlet 20 communicates with the communication pipe 2 through the third con...
Embodiment 3
[0040] Embodiment 3: a multi-mode extraction and solvent distillation recovery storage method for soluble matter in solids, comprising the following steps;
[0041] Distillation recovery and storage of solvents; connect the interface of the connecting pipe with the distillation bottle containing the solvent below, connect the interface of the extraction chamber with the reflux condenser above, and turn the control valve to the point where each reflux pipe is blocked Then heat the distillation bottle, the solvent in the bottle evaporates, the steam enters the extraction chamber from the upper part of the extraction chamber through the connecting pipe and the air guide tube, part of the vapor is condensed by the surrounding wall of the extraction chamber into a liquid and flows into the extraction chamber, and part of the vapor enters the reflux condensing device upwards , is also condensed into a liquid and then returns to the extraction chamber. Since each return pipe is blocke...
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