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A kind of preparation method of self-separating oil silicone rubber

A technology of silicone rubber and compounding rubber, applied in the field of rubber material manufacturing, can solve the problems of high friction system, poor self-lubricating effect and unsuitable application of silicone rubber, and achieve the effect of good mechanical performance and processing performance.

Active Publication Date: 2017-07-11
JIANGSU TIANCHEN NEW MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the friction coefficient of silicone rubber is relatively high, and its self-lubricating effect is not good, so it is not suitable for applications that require lubrication.

Method used

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  • A kind of preparation method of self-separating oil silicone rubber

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Comparison scheme
Effect test

Embodiment 1

[0025] A self-separating oil silicone rubber and a preparation method thereof, the preparation method is as follows; 100 parts of methyl vinyl raw rubber with a vinyl molar content of 0.12% and 3 parts of methyl vinyl raw rubber with a vinyl molar content of 8.0% are added Stir in the kneader, the stirring time is 0.4min; 30 parts of fumed silica, 0.2 parts of stearic acid, and 6 parts of hydroxy silicone oil are added several times respectively, and the number of additions of each component is 4 times. Stir to obtain a silicone rubber compound; after kneading and molding, cool with circulating water and stir for one hour; stir for heating, heat up to 150°C, heat for 2 hours, then vacuumize, and the vacuum pressure is 0.09Mpa; Cool down to 80°C with cooling water to produce glue; after cooling for 12 hours, put the rubber material into a kneader, add 8 parts of phenyl silicone oil, stir for 0.5h, and produce glue; after the glue is produced, cool to room temperature to obtain t...

Embodiment 2

[0028] A self-separating oil silicone rubber and a preparation method thereof, the preparation method is as follows; 100 parts of methyl vinyl raw rubber with a vinyl molar content of 0.12% and 6 parts of methyl vinyl raw rubber with a vinyl molar content of 8.0% are added Stir in a kneader, the stirring time is 0.4min; add 50 parts of fumed silica, 0.4 parts of stearic acid, and 10 parts of hydroxyl silicone oil for multiple times, and the number of additions of each component is 4 times. Stir to obtain a silicone rubber compound; after kneading and molding, cool with circulating water and stir for 1.5 hours; stir for heating, heat up to 150°C, heat for 2 hours, then vacuumize, and the vacuum pressure is 0.06Mpa; Cool down to 80°C with cooling water to produce glue; after cooling for 12 hours, put the rubber material into the kneader, add 10 parts of phenyl silicone oil, stir for 0.5h, and then produce glue; after the glue is produced, cool to room temperature to obtain the pr...

Embodiment 3

[0031] A self-separating oil silicone rubber and a preparation method thereof, the preparation method is as follows; 100 parts of methyl vinyl raw rubber with a vinyl molar content of 0.12% and 5 parts of methyl vinyl raw rubber with a vinyl molar content of 8.0% are added Stir in a kneader for 0.4 minutes; add 35 parts of fumed silica, 0.4 parts of stearic acid and 9 parts of hydroxyl silicone oil for multiple times, the number of additions of each component is 4 times, and stir thoroughly after each addition , to obtain a silicone rubber compound; after kneading and molding, cool with circulating water and stir for 1.5 hours; stir for heating, heat up to 150 ° C, heat for 2 hours, vacuumize, and the vacuum pressure is 0.06Mpa; The cooling water is cooled to 80°C to produce glue; after cooling for 12 hours, put the rubber material into a kneader, add 9 parts of phenyl silicone oil, stir for 0.5h, and produce glue; after the glue is produced, cool to room temperature to obtain ...

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Abstract

The invention discloses a self-separating oil silicone rubber and a preparation method thereof. The self-separating oil silicone rubber of the invention adopts raw rubber with a vinyl molar content of 0.12%, raw rubber with a vinyl molar content of 8.0%, and fumed white carbon black. , phenyl silicone oil, hydroxy silicone oil, stearic acid and other raw materials are kneaded by a kneader. The self-analyzing oil silicone rubber of the present invention has a good self-analyzing oil lubricating effect, and also has better mechanical properties and processing properties, and its application range is wider.

Description

technical field [0001] The invention relates to the manufacture of silicone rubber materials, in particular to a self-separating oil silicone rubber and a preparation method thereof, belonging to the field of rubber material manufacture. Background technique [0002] Silicone rubber has many excellent properties such as good high and low temperature resistance, ozone resistance, weather resistance, insulation and production inertia, and is widely used in various fields of the national economy. However, the friction coefficient of silicone rubber is relatively high, and its self-lubricating effect is not good, so it is not suitable for application in fields that require lubrication. Therefore, the study of self-analyzing oil silicone rubber has very positive significance. Contents of the invention [0003] The purpose of the present invention is to overcome the defects in the prior art, and provide a self-analyzing oil silicone rubber and a preparation method thereof. The ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L83/07C08L83/06C08L83/04C08K3/36C08K5/09
Inventor 徐文俊施贤斌耿政王睿
Owner JIANGSU TIANCHEN NEW MATERIALS