Electronic cigarette liquid with ambergris aroma and preparation method thereof
A technology of e-cigarette liquid and ambergris, which is applied in the field of e-cigarettes, can solve problems such as the large gap, the difficulty in the distribution of aroma components of tobacco extracts, and the fact that the aroma and quality of e-cigarettes cannot meet physiological needs, etc. The demand for aroma, the effect of enriching the flavor of smoking
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Embodiment 1
[0030] Select 2g each of Datobacco leaves from Huidong County, Huili County, Puge County, Panzhihua County, and Xiangyun County in Yunnan Province, dry them in an oven at 40°C, and crush them into tobacco powder with a grinder; add the tobacco powder to 50mL Dichloromethane, ultrasonic extraction for 10min, then let stand for 2h, filter off the smoke dust, collect the organic phase, add 50mL of dilute sulfuric acid with a concentration of 5% to the organic phase, add in two times, collect the water phase; Adjust the pH value to 8, add food-grade ethyl acetate for extraction, separate the organic phase, and then concentrate the organic phase to 1mL to obtain a tobacco extract solution;
[0031] Benzyl alcohol, phenylethyl alcohol, linalool, geraniol, 5-hydroxymethylfurfural, damascenone, β -Dihydrodamascone, β-ionone, and 2-acetylfuran are configured into a solution (dissolved in ethanol) with a total mass concentration of 20%, and the tobacco essence solution is made;
[0032...
Embodiment 2
[0036] Select 10g of Datobacco leaves from Huidong County, Huili County, Puge County, Panzhihua, and Xiangyun County in Yunnan Province, dry them in an oven at 42°C, and crush them into tobacco powder with a grinder; add the tobacco powder to 100mL Dichloromethane, ultrasonic extraction for 20min, then let stand for 2h, filter off the smoke dust, collect the organic phase, add 70mL of dilute sulfuric acid with a concentration of 5% to the organic phase, add in two times, collect the water phase; Adjust the pH value to 9, add food-grade ethyl acetate for extraction, separate the organic phase, and then concentrate the organic phase to 2mL to obtain a tobacco extract solution;
[0037] Benzyl alcohol, phenylethyl alcohol, linalool, geraniol, 5-hydroxymethylfurfural, damascenone, β - Damascone, β-ionone, and 2-acetylfuran are configured into a solution (dissolved in ethanol) with a total mass concentration of 40% to obtain a tobacco essence solution;
[0038] According to the mass...
Embodiment 3
[0042] Select 20g of red tabaco leaves from Huidong County, Huili County, Puge County, Panzhihua, and Xiangyun County in Yunnan, dry them in an oven at 45°C, and crush them into tobacco powder with a grinder; add the tobacco powder to 150mL Dichloromethane, ultrasonic extraction for 25min, then let stand for 2h, filter off the smoke, collect the organic phase, add 80mL of dilute sulfuric acid with a concentration of 5% to the organic phase, add in two times, collect the water phase; Adjust the pH value to 10, add food-grade ethyl acetate for extraction, separate the organic phase, and then concentrate the organic phase to 5mL to obtain a tobacco extract solution;
[0043] Benzyl alcohol, phenylethyl alcohol, linalool, geraniol, 5-hydroxymethylfurfural, β-dihydrodamascone, β- Ionone is configured into a solution (dissolved in ethanol) with a total mass concentration of 50% to obtain a tobacco essence solution;
[0044] According to the mass fraction ratio of 1:10, ambroxol and...
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