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Device and method for adjusting sample scattering plane of a cold neutron triaxial spectrometer

A technique for adjusting devices and neutrons, which is applied in materials analysis using radiation diffraction, etc., which can solve the problems of lack of accuracy, high efficiency, and waste of neutron beam time in the scattering plane of the sample.

Active Publication Date: 2017-05-17
RENMIN UNIVERSITY OF CHINA
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  • Abstract
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  • Claims
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Problems solved by technology

[0003] The first cold neutron triaxial spectrometer in China is built on the cold neutron beamline of the reactor of the Chinese Academy of Engineering. Like the sample stage of the existing international cold neutron triaxial spectrometer, it provides two The rotary θ rotation stage and 2θ rotation stage, and two tilting stages are installed on the sample stage, which lacks accuracy and efficiency in terms of the adjustment of the sample scattering plane, resulting in the sample being placed behind the two inclined stages on the sample stage for the first time. , it is necessary to manually adjust or re-fix the sample near the sample stage by experience, and gradually adjust the scattering plane of the sample to an acceptable error range, which not only wastes a lot of neutron beam time, but also makes the experiment Personnel were repeatedly exposed to residual radiation

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  • Device and method for adjusting sample scattering plane of a cold neutron triaxial spectrometer

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Embodiment Construction

[0015] The present invention will be described in detail below in conjunction with the accompanying drawings and embodiments.

[0016] Such as figure 1 Shown, the adjusting device of the sample scattering plane of the cold neutron three-axis spectrometer of the present invention, it comprises a rotary table 1, a lift table 2, an upper inclined table 3, a lower inclined table 4, four cylindrical pins 5, A circular support plate 6 and a host computer.

[0017] The rotary table 1 is used to adjust the rotation angle of the sample holder around the z-axis, and it includes a rotary table mount 11, a rotary table 12, a first rotating mechanism (not shown), a first stepping motor 13 and a first encoder 14. The top of the rotating table fixing base 11 is fixedly connected to the rotating table 12 through the first rotating mechanism, and the center of the top of the rotating table 12 is provided with a mounting hole for fixing the sample holder. The size of the mounting hole in the e...

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Abstract

The invention relates to a device and a method for adjusting the sample scattered plane of a cold neutron triple-axis spectrometer. The device comprises a rotary table, a lifting table, an upper tilt table, a lower tilt table, round pins, a circular support plate and an upper computer, wherein the rotary table is fixed on the lifting table through one round pin; the lifting table is fixed on the upper tilt table through one round pin; the upper tilt table is fixed on the lower tilt table through one round pin; the lower tilt table is fixed on the circular support plate through one round pin; the circular support plate is fixed on the sample table of the cold neutron triple-axis spectrometer through a location round pin and a screw; the location round pin ensures the superposition of the central axis EE' of the circular support plate and the z-directional central axis of the sample table; the sample table provides a theta rotary table and a 2theta rotary table rotating around the central axis EE' of the circular support plate; the theta rotary table drives the circular support plate to rotate, the 2theta rotary table drives a detector to rotate, and the detector is used for recording the intensity of the outgoing neutrons of a sample and sending the recorded result to the upper computer.

Description

technical field [0001] The invention relates to the technical field of neutron scattering, in particular to a device and method for adjusting a sample scattering plane of a cold neutron triple axis spectrometer. Background technique [0002] Neutron scattering techniques are fully realized by different types of neutron scattering spectrometers. Neutron scattering follows the Ewald sphere in reciprocal vector space, satisfying in, is the incident neutron beam vector, is the outgoing neutron beam vector, is the scattering wave vector. By changing and the size of and direction can be measured and Scattering wave vectors of different sizes and directions in the formed plane all measurable The composed plane is called the scattering plane. For a cold neutron triaxial spectrometer, and are vectors in the horizontal plane, so It must also be located in the horizontal plane, which means that only the scattering vector in the horizontal plane can be measu...

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N23/20
Inventor 张红霞刘娟娟程鹏鲍威
Owner RENMIN UNIVERSITY OF CHINA
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