Varnish and method of making the same
A technology of varnish and bio-oil, applied in coating and other directions, can solve the problems of high soybean oil price and high ink cost, and achieve the effect of low cost and low price
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[0033] The preparation method of above-mentioned varnish comprises the following steps:
[0034] Step S110, by mass percentage, mixing 9%-15% of the first bio-oil and 40%-50% of the second bio-oil and heating to 135°C-145°C to obtain mixed bio-oil.
[0035] Preferably, the first bio-oil and the second bio-oil are added into the reactor and heated with stirring.
[0036] Step S120, under stirring, add 40%-50% petroleum resin to the mixed bio-oil in stages until the petroleum resin is completely dissolved, heat up to 155°C-165°C and keep it warm for 1-1.5 hours before use No more than 5% of the first bio-oil adjusts the varnish with a viscosity of 5000mpa.s-12000mpa.s (25°C).
[0037] Preferably, the petroleum resin is added into the mixed bio-oil three times.
[0038] Step S130, filtering the obtained varnish at 80° C. to 100° C. to make the fineness of the varnish ≤ 15 microns.
[0039] Further, bag filters are used for filtration.
[0040] Preferably, the obtained varnish...
Embodiment 1
[0045] 1. Preparation of varnish
[0046] Weigh 40g of the second bio-oil and 9g of the first bio-oil, put them into the reactor and slowly heat to 140°C, start stirring and keep heating, then slowly put 51g of Shandong Qilong C9-120 petroleum resin into the reactor in three times , observe whether the resin is completely dissolved, and keep it warm at 160°C for 1.5 hours after it is completely dissolved. After sampling and testing all indicators are qualified, wait for the temperature to drop to 100°C and filter the material with 80 mesh.
[0047] Formula Table
[0048] name
Model / Product Name
mass (g)
factory
first bio oil
fatty acid methyl ester
9
Jiangxi Dongfang Julong Chemical Co., Ltd.
Second bio oil
noire
40
Qingyuan Zhonghan New Energy Co., Ltd.
C9-120
51
Shandong Qilong Chemical Co., Ltd.
[0049] Varnish test results:
[0050] project
Tes...
Embodiment 2
[0058] 1. Preparation of varnish
[0059] Weigh 47.2g of the second bio-oil and 9.8g of the first bio-oil, put them into the reaction kettle and slowly heat to 135°C, start stirring and keep heating, and then slowly add 43g of Shandong Qilong C9-120 petroleum resin into the reaction in three times In the kettle, observe whether the resin is completely dissolved. After it is completely dissolved, keep it warm at 155°C for 1.5 hours. After sampling and testing all indicators are qualified, wait for the temperature to drop to 80°C and filter the material with 80 mesh.
[0060] Formula Table
[0061] name
[0062] petroleum resin
[0063] Varnish test results:
[0064] project
[0065] 2. Preparation of black ink
[0066] Weigh 64.5g of varnish at a temperature of 60°C, 1g of Shanghai Sanzheng CH-5 dispersant, and 0.5g of Bentonite38 organobentonite into the batching kettle and stir for 30 minutes, then slowly add 20.5g of Maoming Huanxing N330 carb...
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