Magnetic remediation material for organic pollution in soil or water, preparation method and application
A technology for remediating materials and organic matter, which is applied in the field of soil/water pollution control to achieve the effects of good ecological compatibility, high stability and catalytic activity
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Embodiment 1
[0025] (1) kaolin is standby after drying, pulverizing and crossing 20 mesh sieve pretreatments;
[0026] (2) Add the sieved kaolin into ferrous sulfate and ferric sulfate solution, the theoretical mass ratio of iron oxide to kaolin is 0.5, the molar ratio of ferrous sulfate and ferric sulfate is 2, and the total iron content is 0.5 mol / L for the preparation of iron salt solution. Add 0.5% manganese chloride of total iron mass. The temperature of the suspension was raised to 60°C and continued to stir for 1 hour to stabilize, adding 5 mol / L of sodium hydroxide to raise the pH value of the solution to 9, and continued to stir for 1 hour;
[0027] (3) After the solid precipitate is separated, dried, and pulverized, heat treatment in air at 5°C / min to 400°C for 12 hours to obtain a magnetically separable organic pollution restoration material;
[0028] (4) The above-mentioned magnetic restoration material is added in the mud of polycyclic aromatic hydrocarbon contaminated soil ...
Embodiment 2
[0030] (1) bentonite is standby after drying, pulverizing and crossing 10 mesh sieve pretreatments;
[0031] (2) Add the sieved bentonite to ferrous sulfate and ferric sulfate solution, the theoretical mass ratio of iron oxide to bentonite is 0.1, the molar ratio of ferrous sulfate to ferric sulfate is 0.5, and the total iron content is 0.1 mol / L for the preparation of iron salt solution. Add 0.1% cobalt chloride by mass of total iron. The temperature of the suspension was raised to 30°C and continued to stir for 0.5 hours to stabilize, adding 1 mol / liter of ammonia water to raise the pH value of the solution to 8, and continued to stir for 0.5 hours;
[0032] (3) After the solid precipitate is separated, dried, and pulverized, heat treatment in air at 1°C / min to 200°C for 1 hour to obtain a magnetically separable organic pollution restoration material;
[0033](4) Add the above-mentioned magnetic restoration material to o-(p) chloronitrobenzene polluted water by 0.5wt%, the...
Embodiment 3
[0035] (1) illite is standby after drying, pulverizing and crossing 10 mesh sieve pretreatments;
[0036] (2) Add the sieved illite into ferrous sulfate and ferric sulfate solution, the theoretical mass ratio of iron oxide and illite is 1, the molar ratio of ferrous sulfate and ferric sulfate is 3, and the total iron content The iron salt solution was prepared at 5 mol / L. Add 5% aluminum sulfate of total iron mass. The temperature of the suspension was raised to 90°C and continued to stir for 5 hours to stabilize, adding 10 mol / L of potassium hydroxide to raise the pH value of the solution to 11, and continued to stir for 2 hours;
[0037] (3) After the solid precipitate is separated, dried, and pulverized, heat treatment at 10°C / min to 500°C in air for 24 hours to obtain a magnetically separable organic pollution restoration material;
[0038] (4) Add the above-mentioned magnetic repair material to the mud of petroleum hydrocarbon contaminated soil by 10wt%, the initial pH ...
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