Liquid crystal aligning agent and liquid crystal display element using the same
A technology of liquid crystal aligning agent and liquid crystal aligning film, which is applied in the directions of instruments, coatings, optics, etc., can solve the problems of no covalent bond formation and insufficient substrate bonding, and achieves improved adhesion without reducing liquid crystal alignment. Effect
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[0202] Examples are given below to further describe the present invention in detail. However, the present invention is not limitedly interpreted by these Examples. The abbreviations of the compounds used are shown below.
[0203] NMP: N-methyl-2-pyrrolidone GBL: γ-butyrolactone
[0204] BCS: Butyl Cellosolve IPA: 2-Propanol
[0205] NEP: N-ethyl-2-pyrrolidone PB: Propylene glycol monobutyl ether
[0206] DA-2: a compound represented by the following formula (DA-2)
[0207] DA-3: a compound represented by the following formula (DA-3)
[0208] DA-4: a compound represented by the following formula (DA-4)
[0209] DA-5: p-phenylenediamine
[0210] DA-6: 3,5-Diaminobenzoic acid
[0211] DA-7: 4,4’-Diaminodiphenylmethane
[0212] DA-8: 4,4’-Diaminodiphenylamine
[0213] DA-9: 1,3-bis(4-aminophenoxy)propane
[0214] DA-10: 1,5-bis(4-aminophenoxy)pentane
[0215] DA-11: a compound represented by the following formula (DA-11)
[0216] DA-12: a compound represented by the fo...
Synthetic example 1
[0262] Measure 2.92g (27.0mmol) of diamine DA-5 and 0.71g (3.0mmol) of diamine DA-2 into a 100mL four-necked flask equipped with a stirring device and a nitrogen gas inlet tube, add 81.76g of NMP, and stir while feeding nitrogen gas to dissolve it. While stirring this diamine solution, 6.46 g (28.8 mmol) of carboxylic dianhydride DC-1 was added, and further, NMP was added so that the solid content concentration became 10% by mass, and stirred at room temperature for 4 hours to obtain a polyamic acid solution (PAA-1). The viscosity of this polyamic acid solution at a temperature of 25° C. was 230 mPa·s. In addition, the molecular weight of this polyamic acid was Mn=11,131, Mw=30,009.
Synthetic example 2
[0264] Measure 2.27g (21.0mmol) of diamine DA-5 and 2.69g (9.0mmol) of diamine DA-4 into a 100mL four-neck flask equipped with a stirring device and a nitrogen gas inlet tube, add 61.87g of NMP, and stir while feeding nitrogen gas to dissolve it. While stirring this diamine solution, 5.59 g (28.5 mmol) of carboxylic dianhydride DC-2 was added, and further, NMP was added so that the solid content concentration became 12% by mass, and the polyamic acid was obtained by stirring at room temperature for 4 hours. solution (PAA-2). The viscosity of the polyamic acid solution at a temperature of 25° C. was 410 mPa·s. In addition, the molecular weight of this polyamic acid was Mn=9,042, Mw=19,958.
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