Bile acid components and medicinal uses of bear bile
A technology of bear bile and active ingredients, applied in the field of bile acid components and the medical use of bear bile
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Embodiment 1
[0045] Example 1 Antidepressant Pharmacodynamic Study of Bear Bile
[0046] Material:
[0047] Bear bile powder sample source: Heilongjiang Heibao Pharmaceutical Co., Ltd., batch number: 150516+20141112.
[0048] method:
[0049] 1. Establishment and administration of chronic unpredictable stress depression mouse model
[0050] Four-week-old male C57BL / 6 mice were adaptively fed for two weeks after purchase, and were randomly divided into blank control group, model group, positive drug group (venlafaxine 12.5 mg / kg), bear bile powder low-dose group (low 0.05g / kg), bear bile powder middle dose group (middle0.1g / kg), bear bile powder high dose group (high 0.2g / kg), 12 to 16 animals in each group. The mice in the blank group were reared normally with 4 mice per cage, and the mice in the other groups were housed alone in a single cage, and given the following stimuli from time to time every day: ① restraint for 3 hours, ② reverse day and night for 48 hours, ③ fasting for 24 hou...
Embodiment 2
[0056] Example 2 Detection of bile acid components in bear bile and research on antidepressant pharmacodynamics
[0057] 1. Detection of bile acid components in bear bile by UPLC-MS
[0058] 1.1. Standard total ion chromatogram
[0059] Using UPLC-MS full-scan mode to scan the standard, the fingerprint results are as follows: figure 2 .
[0060] Preparation of reference substance solutions: Take 2 mg of each of the 16 bile acid reference substances (Table 1), weigh them accurately, add 1 mL of methanol to dissolve them, and prepare 2 mg / mL solutions of each reference substance. Take an appropriate amount of each reference substance solution, add methanol and mix to make a mixed reference substance solution of 100 μg / mL.
[0061] Table 1
[0062]
[0063] Bear bile powder sample source: Heilongjiang Heibao Pharmaceutical Co., Ltd., batch number: 150516+20141112.
[0064] Chromatographic conditions: chromatographic column is ACQUITY UPLC BEH column (1.7μm, 1.0mm×100mm);...
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