A kind of preparation method for marble polishing liquid
A technique for polishing liquid and marble, which is applied in the direction of polishing compositions containing abrasives, etc., which can solve the problems that the polishing of marble cannot achieve the polishing effect, and achieve excellent polishing performance, high flatness, and good polishing effect
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Embodiment 1
[0022] (1) Preparation of liquid A: In the reactor, add deionized water: 56mL, oxalic acid: 14g, sodium pyrophosphate: 1.0g, stir and dissolve, add nano-aluminum nitride: 29g, ultrasonically disperse for 1.5 h, and prepare get liquid A;
[0023] (2) Preparation of liquid B: In the reactor, add deionized water: 65 mL, water-soluble cerium salt: 35 g, stir and dissolve to prepare liquid B;
[0024] (3) AlN-CeO 2 Preparation of the complex: under stirring, add 50 mL of liquid B to 50 mL of liquid A, continue to stir, add ammonia water to adjust the pH to 8.0, react for 4 hours, centrifuge, wash with water until neutral, and dry the solid at 110°C. Calcined at 950°C for 6h, cooled, and crushed by airflow to obtain AlN-CeO 2 Composite, the particle size of the composite is 1.0~10μm;
[0025] (4) Preparation of marble polishing solution: In the reactor, add deionized water: 52 mL, acid anhydride: 1.0 g, polyethylene glycol: 1.0 g, AlN-CeO 2 Compound: 46g, stirred, and adjusted t...
Embodiment 2
[0027] (1) Preparation of liquid A: In the reactor, add deionized water: 60mL, oxalic acid: 10g, sodium pyrophosphate: 0.5g, stir and dissolve, add nano-aluminum nitride: 30g, ultrasonically disperse for 1.0h, and prepare get liquid A;
[0028] (2) Preparation of liquid B: In the reactor, add deionized water: 60 mL, water-soluble cerium salt: 40 g, stir and dissolve to prepare liquid B;
[0029] (3) AlN-CeO 2 Preparation of the complex: under stirring, add 55 mL of liquid B to 50 mL of liquid A, continue to stir, add ammonia water to adjust the pH to 8.5, react for 3 hours, centrifuge, wash with water until neutral, and dry the solid at 110°C. Calcined at 980°C for 5h, cooled, and crushed by air flow to obtain AlN-CeO 2 Composite, the particle size of the composite is 1.0~10μm;
[0030] (4) Preparation of marble polishing solution: In the reactor, add deionized water: 48 mL, acid anhydride: 2.0 g, polyethylene glycol: 2.0 g, AlN-CeO 2 Compound: 48g, stirred, and adjusted t...
Embodiment 3
[0032] (1) Preparation of liquid A: In the reactor, add deionized water: 52mL, oxalic acid: 12g, sodium pyrophosphate: 1.0g, stir and dissolve, add nano-aluminum nitride: 35g, ultrasonically disperse for 2.0 h, and prepare get liquid A;
[0033] (2) Preparation of liquid B: In the reactor, add deionized water: 70 mL, water-soluble cerium salt: 30 g, stir and dissolve to prepare liquid B;
[0034] (3) AlN-CeO 2 Preparation of the complex: under stirring, add 60 mL of liquid B to 50 mL of liquid A, continue to stir, add ammonia water to adjust the pH to 9.0, react for 5 hours, centrifuge, wash with water until neutral, and dry the solid at 110°C. Calcined at 1000°C for 4 hours, cooled, and then crushed by airflow to obtain AlN-CeO 2 Composite, the particle size of the composite is 1.0~10μm;
[0035](4) Preparation of marble polishing solution: In the reactor, add deionized water: 58 mL, anhydride: 0.5g, polyethylene glycol: 0.5g, AlN-CeO 2 Compound: 41g, stirred, and adjuste...
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