Gas chromatograph for measuring solution gas in transformer oil

A technology of gas chromatograph and transformer oil, which is applied in the field of gas chromatograph, can solve the problems of long instrument stability time, increased analysis time, and failure to meet the detection limit requirements, and achieve the effect of convenient operation and low cost

Active Publication Date: 2016-11-16
SHANGHAI MUNICIPAL ELECTRIC POWER CO +2
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Problems solved by technology

With a hydrogen flame ionization detector C 2 h 2 The minimum detection limit is 0.1ppm, which cannot meet the detection limit requirements, and there is a problem of mutual influence between sample gases, C 3 + The problem that the components cannot be backflushed, the analysis time is increased, and the stability time of the instrument is too long (generally more than 8 hours)

Method used

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  • Gas chromatograph for measuring solution gas in transformer oil
  • Gas chromatograph for measuring solution gas in transformer oil
  • Gas chromatograph for measuring solution gas in transformer oil

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Embodiment Construction

[0014] According to attached figure 1 , the present invention is a gas chromatograph for measuring dissolved gas in transformer oil, including residual sample gas self-cleaning system, C in transformer oil 3 + Component backflush system, instrument rapid stabilization system and a helium ionization detector (PDD detector)8. The residual sample gas self-cleaning system is provided with an electromagnetic switching valve 3 for controlling the flow rate of the carrier gas. C in the transformer oil mentioned 3 + The component backflushing system includes a ten-way valve 1 on which a quantitative tube 5 and a needle valve 7 are arranged, and the instrument rapid stabilization system includes a four-way valve 2 . The electromagnetic switching valve 3 is connected to the sample injector 4 and then connected to the ten-way valve 1, the helium ionization detector 8, and the four-way valve 2 in sequence. The electromagnetic switch valve 3 is provided with a time controller, which is ...

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Abstract

The invention relates to a gas chromatograph for measuring solution gas in transformer oil. The gas chromatograph is characterized by comprising a residual sample gas self-cleaning system, a back flushing system for C3+ component in transformer oil, an instrument quick stabilizing system and a helium ionization detector, wherein an electromagnetic switch valve used for controlling a gas carrying flow is arranged on the residual sample gas self-cleaning system; the back flushing system for C3+ component in transformer oil comprises a ten-way valve; a quantifying pipe and a needle valve are arranged on the ten-way valve; the instrument quick stabilizing system comprises a four-way valve; the electromagnetic switch valve is connected with a sample injector and then is successively connected with the ten-way valve, the helium ionization detector and the four-way valve. The gas chromatograph for measuring solution gas in transformer oil is low in cost and convenient in operation; the limit of detection can reach 10ppb level; the problems of mutual influences of sample gases and test interference caused by other impurities in gas extruded from the oil can be solved; the stabilizing time of the instrument basically can be controlled within 1 hour.

Description

technical field [0001] The invention relates to a gas chromatograph, and in particular discloses a helium ionization gas chromatograph specially used for measuring transformer oil. Calculate the gas concentration in the transformer oil. Background technique [0002] At present, there are a large number of ultra-high voltage transformers built in China. Due to the high voltage, small discharges and overheating can easily cause major accidents. Therefore, higher requirements are put forward for the detection of dissolved gases in transformer oil. With a hydrogen flame ionization detector C 2 h 2 The minimum detection limit is 0.1ppm, which cannot meet the detection limit requirements, and there is a problem of mutual influence between sample gases, C 3 + The problem that the components cannot be backflushed, the analysis time is increased, and the stability time of the instrument is too long (generally more than 8 hours). Contents of the invention [0003] The purpose of...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/64G01N30/02
CPCG01N30/02G01N30/64G01N2030/025
Inventor 邓先钦彭伟厉敏宪熊鸣翔王祥科潘锐庄鸿涛杨康方华
Owner SHANGHAI MUNICIPAL ELECTRIC POWER CO
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