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A method and device for producing diammonium phosphate from wastewater containing nitrogen and phosphorus

A technology of diammonium phosphate and monoammonium phosphate, which is applied in the directions of phosphate and phosphorus oxyacid, can solve the problems of large waste of resources, high environmental protection treatment costs, and insufficient recycling of nitrogen and phosphorus, so as to improve recycling and utilization. rate, the effect of achieving water balance

Active Publication Date: 2019-01-29
YIDU XINGFA CHEM COMPANY
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  • Summary
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Problems solved by technology

[0002] In the process of producing monoammonium phosphate products by the slurry method, a large amount of wastewater containing nitrogen and phosphorus will be produced. The general treatment method is to transport the wastewater to the sewage treatment station for treatment and then discharge it up to the standard. The cost of environmental protection treatment is high, and the nitrogen in the wastewater , Phosphorus has not been effectively recycled, resulting in a large waste of resources

Method used

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  • A method and device for producing diammonium phosphate from wastewater containing nitrogen and phosphorus

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Embodiment Construction

[0022] As shown in the figure, the present invention will be further described in conjunction with the accompanying drawings:

[0023] Adopt the present invention to produce diammonium phosphate product as diammonium lotion by reclaiming nitrogen-containing phosphorus waste water, concrete scheme is as follows:

[0024] The specific steps are as follows:

[0025] 1. Send nitrogen and phosphorus-containing waste water to the tail gas scrubber 1 of diammonium phosphate, and circulate through the tail washing circulation pump 2 in the tail washing Venturi scrubber 13 to wash and absorb the tail gas of the diammonium plant.

[0026] 2. The tail gas washing circulating liquid is transported to the scrubber tank 3 through the tail gas washing pump 2, the concentrated phosphoric acid and the tail washing circulating liquid are interlocked and added into the scrubber 12, and the concentrated phosphoric acid and the tail washing circulating liquid are separated under the agitation of t...

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Abstract

The invention discloses a method for producing diammonium phosphate with nitrogen and phosphorus containing wastewater. The method specifically includes: delivering the nitrogen and phosphorus containing wastewater produced in production of monoammonium phosphate to a diammonium phosphate exhaust scrubber to serve as lotion filling water to scrub and adsorb exhaust from a diammonium phosphate production plant; delivering diammonium phosphate exhaust scrubbing cyclic liquid to the scrubber to be mixed proportionally with concentrated phosphoric acid to adsorb dust and ammonia containing exhaust gas from the main line of the diammonium phosphate production plant; delivering the concentrated phosphoric acid and scrubber lotion to a tubular reactor reservoir to be mixed with acid to reach proportion and neutralization required by a diammonium-phosphate tubular reactor; feeding the mixed acid with appropriate proportion to the tubular reactor to react with liquid ammonia to generate slurry to be injected rapidly to a granulating machine layer for granulation. The diammonium phosphate product is produced by recycling the nitrogen and phosphorus containing wastewater generated from the diammonium phosphate production plant, annual recycling of P2O5 is 163 tons, annual recycling of nitrogen is 12 tons and annual increasing income is 610 thousand RMB Yuan according to consumption of nitrogen and phosphorus wastewater of 12 m<3> / hour.

Description

technical field [0001] The present invention relates to sewage treatment, and at the same time relates to the recycling and utilization of nitrogen and phosphorus resources. Specifically, the waste water containing nitrogen and phosphorus produced in the production process of monoammonium phosphate is recycled for diammonium phosphate lotion replenishment to produce diammonium phosphate products. way. Background technique [0002] In the process of producing monoammonium phosphate products by the slurry method, a large amount of wastewater containing nitrogen and phosphorus will be produced. The general treatment method is to transport the wastewater to the sewage treatment station for treatment and then discharge it up to the standard. The cost of environmental protection treatment is high, and the nitrogen in the wastewater , Phosphorus has not been effectively recycled, resulting in a large waste of resources. [0003] At the same time, in the process of producing diammo...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B25/28
CPCC01B25/28
Inventor 彭洪新郑光明邹学勇沈维云刘明高杜万宝朱刚王宗孝
Owner YIDU XINGFA CHEM COMPANY
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