Fermented feed containing humic acid chelated trace elements and preparation method thereof
A technology for chelating trace elements and fermented feed, which is applied to animal feed, animal feed, bacteria used in food preparation, etc. Cost, boosting immunity, changing the effect of medicinal properties
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Embodiment 1
[0041] Embodiment 1: Chelation process research of trace element and humic acid
[0042] 1. Chelation of humic acid and zinc
[0043] The specific chelation method is as follows:
[0044] Combine humic acid (fulvic acid, commercially available product) with Zn 2+ According to the molar ratio of 1:1 (1kg humic acid: 50g ZnSO 4 ·7H 2 (0) was added into 50L of water to adjust the pH to 5, and reacted for 1 hour at 80° C. under stirring conditions to obtain a zinc humate chelate solution. Then concentrate the zinc humate chelating solution at 60°C, take it out when the chelating solution is thick but not hard, add (multiple times) 100L of absolute ethanol and stir to mix evenly, to wash and remove free zinc , discard the supernatant by centrifugation, and completely dry the precipitate in an oven to obtain zinc humate chelate.
[0045] Adopt atomic absorption spectrophotometry to measure the chelation rate of chelate, concrete method is:
[0046] Atomic absorption spectropho...
Embodiment 2
[0061] Example 2: Preparation of fermented feed containing humic acid chelated trace elements
[0062] 1. Composition of fermentation medium:
[0063] 55% fermented material, 45% water; all are percentages by mass.
[0064] The composition of the fermented material is:
[0065] 15 parts of soybean meal, 35 parts of bran, 8 parts of humic acid, 45 parts of stone powder, 8 parts of chrysanthemum, 6 parts of silver thread grass, 6 parts of apocynum leaves, 5 parts of golden gentian, 5 parts of cloth dregs leaves, humic acid Chelated trace elements 1 part.
[0066] Among them, humic acid chelated trace elements are mixed with zinc humate, copper humate and manganese humate at a mass ratio of 2:0.1:8.
[0067] The above-mentioned zinc humate, copper humate and manganese humate were prepared according to the chelation method of Example 1.
[0068] 2. The preparation method is as follows:
[0069] (1) Dried, pulverized, and mixed to make traditional Chinese medicine powder;
[...
Embodiment 3
[0072] Example 3: Preparation of fermented feed containing humic acid chelated trace elements
[0073] 1. The composition of the fermentation medium:
[0074] 60% fermented material, 40% water; all are percentages by mass.
[0075] The composition of the fermented material is:
[0076] 10 parts of soybean meal, 45 parts of bran, 5 parts of humic acid, 50 parts of stone powder, 5 parts of chrysanthemum, 10 parts of silvergrass, 4 parts of apocynum leaves, 8 parts of golden gentian, 4 parts of cloth dregs leaves, humic acid Chelated trace elements 0.7 parts.
[0077] Wherein, the humic acid chelated trace element is formed by mixing zinc humate, copper humate and manganese humate in a mass ratio of 3.6:0.215:10.
[0078] The above-mentioned zinc humate, copper humate and manganese humate were prepared according to the chelation method of Example 1.
[0079] 2. The preparation method is as follows:
[0080] (1) Dried, pulverized, and mixed to make traditional Chinese medicin...
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