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Preparation method for quartz glass and quartz glass

A quartz glass, purpose technology, used in glass manufacturing equipment, glass forming, manufacturing tools, etc., can solve the problems of fast corrosion rate, corrosion, and inability to meet the requirements of semiconductor applications.

Active Publication Date: 2017-02-08
CHINA BUILDING MATERIALS ACAD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Si-O chemical bonds are easily corroded by hydrofluoric acid. According to calculations, in the hydrofluoric acid environment, the corrosion rate of quartz glass composed entirely of Si-O chemical bonds has reached 150 μm / h. The corrosion rate is faster in hydrofluoric acid environment, which cannot meet the application requirements of semiconductor etching in hydrofluoric acid environment

Method used

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  • Preparation method for quartz glass and quartz glass
  • Preparation method for quartz glass and quartz glass
  • Preparation method for quartz glass and quartz glass

Examples

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Effect test

preparation example Construction

[0056] like figure 1 Shown, a kind of preparation method of quartz glass that one embodiment of the present invention proposes, it comprises:

[0057] Step 10, using a dissolving agent to dissolve and mix the first doping compound and the second doping compound to form a doping mixed solution, the first doping compound is an aluminum-containing compound, and the second doping compound includes a Zr-containing compound, At least one of Y-containing compounds, La-containing compounds, Sc-containing compounds, Th-containing compounds, V-containing compounds, and Ti-containing compounds;

[0058] Wherein, the dissolving agent can be a kind of dissolving agent, which can dissolve the first doping compound and the second doping compound simultaneously; or, the dissolving agent can include two kinds of dissolving agents, one kind of dissolving agent is used to dissolve the first Doping compound, another dissolving agent is used to dissolve the second doping compound, forming a dopin...

Embodiment approach

[0099] 1. Vacuum electric melting process melting method:

[0100] Grinding the doping batch material, and screening the doping batch material after grinding, to obtain the doping batch material after screening, adopting a melting process for the doping batch material after screening, At 1000-2500 degrees Celsius, it is melted into the finished quartz glass, specifically:

[0101] Sieve the doped batch material after grinding to obtain the doped batch material with particles of 20-200 mesh, and melt the doped batch material with 20-200 mesh by vacuum electric melting process to form the finished quartz glass product.

[0102] 2. High-frequency plasma melting process Melting method:

[0103] Grinding the doping batch material, and screening the doping batch material after grinding, to obtain the doping batch material after screening, adopting a melting process for the doping batch material after screening, At 1000-2500 degrees Celsius, it is melted into the finished quartz gl...

Embodiment 2

[0119] A kind of quartz glass that one embodiment of the present invention proposes, comprises:

[0120] Quartz glass finished product, prepared by the preparation method of said quartz glass finished quartz glass;

[0121] The preparation method of described quartz glass comprises:

[0122]The first doping compound and the second doping compound are dissolved and mixed by a dissolving agent to form a doping mixed solution, the first doping compound is an aluminum-containing compound, and the second doping compound includes a Zr-containing compound and a Y-containing compound , at least one of La-containing compounds, Sc-containing compounds, Th-containing compounds, V-containing compounds, and Ti-containing compounds;

[0123] mixing a silicon-containing raw material with the doping mixture solution to obtain a doping mixture;

[0124] The doped mixture is fired into a finished quartz glass product through a firing process, wherein the finished quartz glass contains Al that...

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Abstract

The invention relates to a preparation method for quartz glass and quartz glass, relates to the technical field of quartz glass manufacturing, and aims at improving corrosion resistance, in fluorine-containing environments such as hydrofluoric acid and fluorine gas F2, of quartz glass finished products. The method comprises the following steps: dissolving and mixing a first doping compound and a second doping compound through a dissolving agent to form a doped mixed solution, wherein the first doping compound is an aluminum-containing compound, the second doping compound is at least one of a Zr-containing compound, a Y-containing compound, a La-containing compound, an Sc-containing compound, a Th-containing compound, a V-containing compound and a Ti-containing compound, and the quartz glass finished product comprises Al2O3 formed by burning and converting a first part, and at least one of ZrO2, Y2O3, La2O3, Sc2O3, ThO2, V2O5 and TiO2 formed by burning and converting a second part; and Al2O3, ZrO2, Y2O3, La2O3, Sc2O3, ThO2, V2O5 and TiO2 are charged into gaps of a SiO2 tetrahedral network structure in the form of a network intermediate or a network exterior body, so that glass quartz is resistant to acidic corrosion.

Description

technical field [0001] The invention relates to the technical field of quartz glass manufacturing, in particular to a method for preparing quartz glass and the quartz glass. Background technique [0002] Quartz glass is an amorphous material with silicon dioxide as the main component. Its microstructure is a simple network composed of silicon dioxide tetrahedral structural units. Because the Si-O chemical bond energy is large and the structure is very tight, so Quartz glass has unique properties, such as high temperature resistance, low expansion coefficient, thermal shock resistance, high chemical stability and good electrical insulation properties. [0003] Due to the unique properties of quartz glass, it is an irreplaceable ideal auxiliary material in the manufacturing process of semiconductor integrated circuits, including quartz glass tubes, quartz glass sheets, quartz glass rings, quartz glass plates, quartz glass flanges, quartz glass groove boats, Quartz glass clean...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C3/06C03C1/02C03C6/08C03B20/00
CPCC03B19/066C03C1/026C03C3/06C03C2201/36
Inventor 聂兰舰向在奎贾亚男王蕾邵竹锋王慧张辰阳符博王玉芬
Owner CHINA BUILDING MATERIALS ACAD