Anti-radiation lead and cadmium free low temperature frit and preparation method thereof
A low-temperature frit and radiation protection technology, applied in the field of ceramics, can solve problems such as containing high toxicity, achieve long-term antibacterial, prevent agglomeration, and improve stability.
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Embodiment 1
[0037] A radiation-proof lead-free cadmium low-temperature frit and a preparation method thereof, the preparation method comprising the following steps:
[0038] A mixing material: mix and grind 12% quartz, 12% feldspar, 15% borax, 6% carbonate, 35% boric acid, 5% spodumene, 4% fluoride salt, 0.9% kaolin, and then add 0.1 % antibacterial compound and 10% anti-radiation compound, grind uniformly to obtain the mixture; the feldspar is obtained by mixing potassium feldspar and albite feldspar in a weight ratio of 4:1; the carbonate is made of potassium carbonate, carbonic acid Sodium, barium carbonate, lithium carbonate and calcium carbonate are mixed in a weight ratio of 3:1:3:2:1; the fluoride salt is obtained by mixing sodium fluoride, calcium fluoride and lithium fluoride in a weight ratio of 4:2: 1 mixed;
[0039] B Melting: Sprinkle the mixture prepared in step A into a refractory sagger, and perform high-temperature melting at 1250~1320°C to obtain a molten slurry; the hi...
Embodiment 2
[0051] A radiation-proof lead-free cadmium low-temperature frit and a preparation method thereof, the preparation method comprising the following steps:
[0052] A mixture: mix and grind 15% quartz, 6% feldspar, 20% borax, 7% carbonate, 25% boric acid, 6% spodumene, 3% fluoride salt, 3% kaolin, and then add 3 % antibacterial compound and 12% anti-radiation compound, grind uniformly and make mixture; Described feldspar is obtained by mixing potassium feldspar and albite feldspar by weight ratio 4:1; Described carbonate is made of potassium carbonate, carbonic acid Sodium, barium carbonate, lithium carbonate and calcium carbonate are mixed in a weight ratio of 3:1:3:2:1; the fluoride salt is obtained by mixing sodium fluoride, calcium fluoride and lithium fluoride in a weight ratio of 4:2: 1 mixed;
[0053] B Melting: Sprinkle the mixture prepared in step A into a refractory sagger, and perform high-temperature melting at 1250~1320°C to obtain a molten slurry; the high-temperatur...
Embodiment 3
[0065] A radiation-proof lead-free cadmium low-temperature frit and a preparation method thereof, the preparation method comprising the following steps:
[0066] A mixture: mix and grind 18% quartz, 5% feldspar, 25% borax, 3% carbonate, 20% boric acid, 3% spodumene, 1% fluoride salt, 5% kaolin, and then add 5 % antibacterial compound and 15% anti-radiation compound, grind uniformly to make mixture; described feldspar is obtained by mixing potassium feldspar and albite feldspar in a weight ratio of 4:1; described carbonate is made of potassium carbonate, carbonic acid Sodium, barium carbonate, lithium carbonate and calcium carbonate are mixed in a weight ratio of 3:1:3:2:1; the fluoride salt is obtained by mixing sodium fluoride, calcium fluoride and lithium fluoride in a weight ratio of 4:2: 1 mixed;
[0067] B Melting: Sprinkle the mixture prepared in step A into a refractory sagger, and perform high-temperature melting at 1250~1320°C to obtain a molten slurry; the high-temp...
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