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A kind of soluble temporary plugging agent for acid fracturing and preparation method thereof

A technology of temporary plugging agent and magnesium alloy, which is applied in the field of temporary plugging agent, can solve the problems of poor control of dissolution time, influence on acidizing fracturing effect, insufficient stability and reliability, etc., and achieve good controllability of dissolution time and plugging effect Stable and reliable, practical effect

Active Publication Date: 2018-12-25
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Polymer temporary plugging agents have low temperature resistance, and the dissolution time is not easy to control. This type of temporary plugging agent is only suitable for oil and gas wells with shallow burial depth and low bottom hole temperature, and cannot be applied to oil and gas wells with burial depths of 4000-8000 m, high-temperature deep wells with a bottom-hole temperature of 120-180°C (however, with the continuous development of oil and gas wells, high-temperature deep wells have become the development direction of oil and gas wells), that is, their application range is limited
Although inorganic salt temporary plugging agents are suitable for acid fracturing operations in high-temperature deep wells due to their high temperature resistance, their plugging performance is poor, not stable and reliable, and will not only affect the effect of acid fracturing, but also cause damage to the reservoir. Big damage, poor practicality

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] The total weight of the present invention is 300g, which is mainly composed of the following soluble raw materials in weight percentage: 90% magnesium alloy pellets, i.e. 270g; 9% magnesium alloy flakes, i.e. 27g; 1% fiber, i.e. 3g. Among them, the particle size of the magnesium alloy pellets is about 90 meshes; the length and width of the magnesium alloy flakes are about 5.0 mm, and the thickness is about 0.4 mm; the fibers are polylactic acid fibers, and the length of the fibers is about 5.0 mm.

[0041] The above-mentioned magnesium alloy pellets and magnesium alloy flakes are respectively taken from magnesium alloy rods (of course, other profiles of magnesium alloys can also be used), the total weight of the magnesium alloy rods is 1000g, and it is mainly formed by melting and casting the raw materials in the following weight percentages : Magnesium powder 92%, that is 920g; aluminum powder 3%, that is 30g; iron powder 5%, that is 50g. Among them, the purity of magn...

Embodiment 2

[0049]The total weight of the present invention is 300g, and it is mainly made up of the soluble raw material of following percentage by weight: 70% of magnesium alloy pellets, namely 210g; 26% of magnesium alloy flakes, namely 78g; 4% of fiber, namely 12g. Among them, the particle size of the magnesium alloy pellets is about 20 meshes; the length and width of the magnesium alloy flakes are about 8.0 mm, and the thickness is about 0.8 mm; the fibers are polylactic acid fibers, and the length of the fibers is about 6.0 mm.

[0050] The above-mentioned magnesium alloy pellets and magnesium alloy flakes are respectively taken from magnesium alloy rods (of course, other profiles of magnesium alloys can also be used), the total weight of the magnesium alloy rods is 1000g, and it is mainly formed by melting and casting the raw materials in the following weight percentages : Magnesium powder 87%, that is 870g; aluminum powder 3%, that is 30g; iron powder 10%, that is 100g. Among them...

Embodiment 3

[0058] The total weight of the present invention is 300g, which is mainly composed of the following soluble raw materials in weight percentage: 60% of magnesium alloy pellets, i.e. 180g; 37% of magnesium alloy flakes, i.e. 111g; 3% of fibers, i.e. 9g. Among them, the particle size of the magnesium alloy pellets is about 60 meshes; the length and width of the magnesium alloy flakes are about 7.0 mm and the thickness is about 0.6 mm; the fibers are polyvinyl alcohol fibers, and the length of the fibers is about 5.0 mm.

[0059] The above-mentioned magnesium alloy pellets and magnesium alloy flakes are respectively taken from magnesium alloy rods (of course, other profiles of magnesium alloys can also be used), the total weight of the magnesium alloy rods is 1000g, and it is mainly formed by melting and casting the raw materials in the following weight percentages : Magnesium powder 90%, that is 900g; aluminum powder 5%, that is 50g; iron powder 5%, that is 50g. Among them, the p...

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Abstract

The invention discloses a soluble temporary plugging agent used for acidizing fracturing, and a preparation method thereof. The soluble temporary plugging agent is mainly composed of following soluble raw materials, by weight, 60 to 90% of magnesium alloy particle, 6 to 39% of magnesium alloy sheet, and 1 to 4% of fiber. The preparation method comprises following steps: 1, magnesium powder, aluminium powder, and iron powder obtained via drying pretreatment are delivered into a smelting furnace at a certain ratio, are heated to 660 to 700 DEG C under protection by an insert gas so as to melt the magnesium powder and the aluminium powder, and are stirred to as to realize uniform mixing of iron powder in an obtained magnesium aluminium melted liquid, an obtained mixture is subjected to thermal insulation for 25 to 35min at 660 to 700 DEG C, and is subjected to casting so as to obtain a bar material, and the bar material is cooled to room temperature; 2, the magnesium alloy bar material is processed into particles and sheets; and 3, the obtained magnesium alloy particle, the magnesium alloy sheet, and fiber are mixed with a carrying fluid at a certain ratio. The soluble temporary plugging agent possesses high temperature resistance, high plugging strength, stable plugging effect, excellent dissolving controllability, and high reliability.

Description

technical field [0001] The invention relates to a temporary plugging agent used in the development of oil and gas wells, in particular to a soluble temporary plugging agent for acid fracturing and a preparation method of the temporary plugging agent. Background technique [0002] Staged fracturing is the main means of increasing production in low-permeability and ultra-low-permeability oil and gas fields. With the large-scale development of horizontal wells, various multi-stage fracturing technologies have been gradually popularized and applied. In order to form more fractures in the reservoir of oil and gas wells during fracturing, so as to increase oil and gas production, it is an important technical measure to switch from temporary plugging to acid fracturing. [0003] Temporary plugging to acid fracturing technology often requires the use of temporary plugging agents to reduce the invasion of working fluids into the reservoir, that is, temporary plugging agents are used ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/504C09K8/50
CPCC09K8/50C09K8/5045C09K2208/08
Inventor 刘多容戚斌兰林龙刚潘宝风李尚贵杨兵孙勇黄贵存王文耀
Owner CHINA PETROLEUM & CHEM CORP
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