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Pentacalcium ascorbate sorbate and preparation method thereof

A technology of ascorbic acid and sorbic acid, which is applied in the field of biochemical medicine, medicine and food, can solve problems such as inability to make eye drops, and achieve the effects of easy operation, prevention of decomposition and simple preparation method.

Inactive Publication Date: 2017-05-24
李玉成
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the calcium ascorbate can supplement calcium and VC at the same time, it cannot be made into eye drops, oral liquids and injections
However, there is no such substance as pentacalcium sorbate in the domestic and foreign markets.

Method used

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  • Pentacalcium ascorbate sorbate and preparation method thereof
  • Pentacalcium ascorbate sorbate and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] The preparation method of present embodiment ascorbate pentacalcium sorbate comprises the following steps:

[0029] (1) Take raw material calcium oxide powder 280.4g, ascorbic acid powder 1585.1g and sorbic acid powder 112.1g, raw material is dropped in the stirring ball mill, start stirring ball mill, carry out chemical reaction under normal temperature, chemical reaction formula is:

[0030] 5CaO+9C 6 h 8 o 6 +C 6 h 8 o 2 = Ca 5 (C 6 h 7 o 6 ) 9 (C 6 h 7 o 2 )·5H 2 O.

[0031] (2) After fully reacting for 40 minutes, stop stirring the ball mill and release the product, and dry the product at a temperature of 105°C;

[0032] (3) The dried product was cooled to room temperature, and weighed after cooling to obtain 1938.1 g of the product pentacalcium ascorbyl sorbate.

[0033] (4) Ascorbate pentacalcium sorbate gained in step (3) is packaged as a finished product.

Embodiment 2

[0035] The preparation method of present embodiment ascorbate pentacalcium sorbate comprises the following steps:

[0036] (1) Take by weighing raw material calcium oxide powder 140.2g, ascorbic acid powder 792.5g and sorbic acid powder 56.1g, raw material is dropped in the stirring ball mill, start stirring ball mill, carry out chemical reaction under normal temperature, chemical reaction formula is:

[0037] 5CaO+9C 6 h 8 o 6 +C 6 h 8 o 2 = Ca 5 (C 6 h 7 o 6 ) 9 (C 6 h 7 o 2 )·5H 2 O.

[0038] (2) After fully reacting for 30 minutes, stop stirring the ball mill and release the product, and dry the product at a temperature of 102°C;

[0039] (3) The dried product was cooled to room temperature, and weighed after cooling to obtain 978.9 g of the product pentacalcium ascorbyl sorbate.

[0040] (4) Ascorbate pentacalcium sorbate gained in step (3) is packaged as a finished product.

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Abstract

The invention relates to a new substance pentacalcium ascorbate sorbate. The chemical molecular formula of the new substance is Ca5(C6H7O6)9(C6H7O2).5H2O, and the molecular weight is 1977.7. A preparation method of the pentacalcium ascorbate sorbate comprises the following steps: 1, adding calcium oxide, ascorbic acid and sorbic acid to a reaction container, and carrying out a chemical reaction; 2, drying the obtained product after the reaction is fully completed; and 3, cooling the dried product to room temperature to obtain the product pentacalcium ascorbate sorbate. The pentacalcium ascorbate sorbate prepared in the invention simultaneously supplements calcium and VC to human bodies, can be used as a calcium and VC supplementing, oxidation preventing and fresh keeping agent, can be used as a calcium and VC supplementing food additive, and can be used for treating osteoporosis, leg cramp, bronchitis and other diseases.

Description

technical field [0001] The invention relates to the field of biochemical medicine and food, in particular to glucose calcium ascorbate and its preparation method and application. Background technique [0002] Calcium Ca is an essential element for the human body. Cationic calcium has the functions of strengthening bones, strengthening teeth, reducing inflammation, analgesia, maintaining normal excitability of nerves and muscles, and treating allergic diseases. [0003] Ascorbate C 6 h 8 o 6 (abbreviated as VC, also known as vitamin C), the main function is to improve immunity, prevent cancer, heart disease, stroke, protect teeth and gums, etc. The reducing property of ascorbic acid can eliminate the nitroso groups that cause cancer and the free radicals that cause aging, so it has the effects of anti-aging, anti-cancer, anti-oxidation, anti-scurvy, anti-fatigue, anti-inflammation, and disinfection. It is a food and condiment Excellent anti-oxidant preservative for bevera...

Claims

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Application Information

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IPC IPC(8): C07D307/62C07C57/10C07C51/41A61K31/375A61P19/10A61P3/14A61P11/00A61P31/16A61P11/06A61P35/00A61P1/16A61P9/12A23L33/16A23L33/15A23L3/3544A61K31/19
CPCC07D307/62A23L3/3544A23V2002/00A61K31/19A61K31/375C07C51/412C07C57/10A61K2300/00A23V2200/02A23V2200/306A23V2250/1578A23V2250/708A23V2250/054
Inventor 李玉成
Owner 李玉成
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