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Wear-resistant protective coating, its preparation method and application

A protective coating and coating technology, applied in the field of wear-resistant protective coating, can solve problems such as lack of research on VCN coating, and achieve the effects of improving comprehensive performance and service life, improving bonding performance, and good application value

Active Publication Date: 2019-07-19
NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Second, there is a relative lack of research on VCN coatings in extremely harsh environments

Method used

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  • Wear-resistant protective coating, its preparation method and application
  • Wear-resistant protective coating, its preparation method and application
  • Wear-resistant protective coating, its preparation method and application

Examples

Experimental program
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preparation example Construction

[0041] Another aspect of the present invention provides a method for preparing the wear-resistant protective coating, see figure 1 Shown, described preparation method comprises:

[0042] S1. Deposition of a hard V transition layer:

[0043] Using arc ion plating technology, a hard V transition layer is deposited on the surface of stainless steel mechanical movement foundation parts and other substrates;

[0044] S2. Deposition of VCN coating:

[0045] Using arc ion plating technology, continue to deposit VCN coating on the surface of the substrate with the hard V transition layer.

[0046] In some embodiments, the step S1 includes: using an arc ion plating system to pre-deposit the hard V transition layer on the surface of the stainless steel mechanical movement base; the target metal V target used, the vacuum degree of the base of the reaction chamber ( 3~6)×10 -3 Pa, the working atmosphere is Ar, the flow rate is 350-450sccm, the working vacuum is 0.2-0.5Pa; the depositi...

Embodiment 1

[0070] The substrate is a stainless steel gear in the mechanical parts, and the specific steps of the preparation method of the wear-resistant protective coating are as follows:

[0071] (1) Pre-plating treatment

[0072] Put the stainless steel gear base in petroleum ether, and clean it with ultrasonic stirring for 30 minutes. After removing the oil stain on the stainless steel surface, put it in acetone and ultrasonically clean it for 20 minutes, then ultrasonically clean it in absolute ethanol for 15 minutes, and finally take it out and dry it with nitrogen;

[0073] (2) Bias reverse sputter cleaning

[0074] Put the above treated stainless steel gear into the chamber, heat the temperature of the reaction chamber to 350°C, and pre-evacuate the back to 4.00×10 -3 Pa. Enter high-purity Ar (purity ≥ 99.99%), flow rate 100sccm, turn on V target (purity ≥ 99.5%) DC power supply, set the target current to 60A, and continuously bombard stainless steel under the bias voltages of ...

Embodiment 2

[0085] The substrate is a stainless steel-based sealing ring in key marine components, and the specific steps of the preparation method of the wear-resistant protective coating are as follows:

[0086] (1) Utilize the method for embodiment 1 step 1 to implement pre-plating treatment to the stainless steel-based sealing ring;

[0087] (2) Utilize the method for embodiment 1 step 2 to implement bias reverse sputtering cleaning to the stainless steel-based sealing ring;

[0088] (3) Utilize the method for embodiment 1 step 3 to deposit hard V transition layer to stainless steel-based sealing ring;

[0089] (4) An arc ion plating system is used to deposit a VCN coating on the surface of the stainless steel-based sealing ring of the above-mentioned deposition V transition layer. The target material used is 6 metal V targets (purity ≥ 99.5%). Under the continuous vacuum coating state, The base vacuum of the reaction chamber is maintained at 4.5×10 -3 Pa, cut off the inflow of Ar, ...

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Abstract

The invention discloses an anti-abrasion protective coating and a preparation method and application thereof. The anti-abrasion protective coating comprises a hard V transition layer covering the surface of a substrate and a VCN coating covering the hard V transition layer. The substrate is preferably selected from stainless steel mechanical motion basic parts. The preparation method comprises the steps that the hard V transition layer is deposited on the surface of the substrate through an arc ion plating technology; and then, the VCN coating is deposited on the hard V transition layer through the arc ion plating technology. According to the anti-abrasion protective coating and the preparation method and application thereof, the VCN coating is mainly composed of a VC phase and a VN phase, is of a classic amorphous inlay nanocrystalline structure, and is low in friction coefficient and abrasion rate in atmosphere and seawater environments; through the hard V transition layer, the bonding property between the substrate, namely, a stainless steel mechanical motion basic part and the VCN coating which are widely different in component can be improved, meanwhile, part of stress in the VCN coating is released, accordingly, the comprehensive performance of the VCN coating and the stainless steel mechanical motion basic part is effectively improved, and the service life of the VCN coating and the service life of the stainless steel mechanical motion basic part are effectively prolonged.

Description

technical field [0001] The invention specifically relates to a wear-resistant protective coating, its preparation method and application, and belongs to the technical field of surface engineering protection. Background technique [0002] The development of the ocean has high requirements for the hardness, strength and fatigue resistance of the base materials of various mechanical parts. Whether the parts of the equipment can work safely and stably for a long time depends largely on the direct friction and wear and medium erosion. Changes in the surface state such as plastic deformation, crack growth, erosion, cavitation, oxidation, and material stripping will lead to a significant reduction in the service life and safety of the part. Even for parts that fail as a whole, the failure process is often It starts from the surface that bears the external action and gradually expands to the core of the material. Under the operating conditions of many mechanical equipment (such as ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C14/06C23C14/16C23C14/32
CPCC23C14/0021C23C14/0664C23C14/16C23C14/325C23C28/322C23C28/34
Inventor 王永欣叶育伟慕永涛姚懿容王立平
Owner NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI