Complex of secondary complex magnesium as well as preparation method and application thereof
A technology of complex compound and complex magnesium, applied in the field of complex compound, can solve the problem that nutrients are not easily absorbed and utilized, and achieve the effects of enhancing antioxidant function, low cost and high biological titer
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Embodiment 1
[0043] A secondary complex of magnesium is prepared from sucrose, magnesium salt and amino acid.
[0044] The preparation method of the complex of described secondary complex magnesium comprises the following steps:
[0045](1) Add 30 parts by weight of sucrose in the reactor, add 50 parts by weight of water to dissolve the sucrose, add 8 parts by weight of magnesium chloride, alkalinize the aqueous solution of sodium hydroxide, adjust the pH of the solution to be 11, heat the reactor, keep The temperature in the kettle is between 70-80°C, and the complexation reaction is carried out for 1 hour. The reaction process is continuously stirred to generate a magnesium sucrose solution, which is filtered and separated to obtain the filter residue A and the filtrate a. Add 2 times the weight of 75% ethanol to the filtrate a The solution is precipitated, and after the precipitation is complete, it is centrifugally filtered to obtain the filter residue B and the filtrate b. The filter ...
Embodiment 2
[0049] A secondary complex of magnesium is prepared from sucrose, magnesium salt and amino acid.
[0050] The preparation method of the complex of described secondary complex magnesium comprises the following steps:
[0051] (1) Add 40 parts by weight of sucrose in the reactor, add 65 parts by weight of water to dissolve the sucrose, add 11 parts by weight of magnesium sulfate, alkalinize the aqueous solution of sodium hydroxide, adjust the pH of the solution to be 12, heat the reactor, Keep the temperature in the kettle between 70-80°C, carry out the complexation reaction for 2 hours, continuously stir during the reaction process, generate sucrose magnesium solution, filter and separate, obtain filter residue A and filtrate a, add 75% of 2 times the weight of filtrate a The ethanol solution is precipitated, and after the precipitation is complete, it is centrifuged and filtered to obtain the filter residue B and the filtrate b. The filter residue B is vacuum-dried and dried, ...
Embodiment 3
[0055] A secondary complex of magnesium is prepared from sucrose, magnesium salt and amino acid.
[0056] The preparation method of the complex of described secondary complex magnesium comprises the following steps:
[0057] (1) Add 35 parts by weight of sucrose in the reactor, add 63 parts by weight of water to dissolve the sucrose, add 10 parts by weight of magnesium oxide, add aqueous sodium hydroxide solution for alkalization, adjust the pH of the solution to be 11, heat the reactor, Keep the temperature in the kettle between 70-80°C, carry out the complexation reaction for 1.5h, continuously stir during the reaction process, generate a sucrose magnesium solution, filter and separate, obtain the filter residue A and filtrate a, add 2 times the weight of 75 % ethanol solution for precipitation, after the precipitation is complete, centrifuge and suction filter to obtain filter residue B and filtrate b, filter residue B is vacuum-dried and dried, sieved and detected, and the...
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