The invention discloses sec-
ethyl phosphate as well as a preparation method and application thereof, and belongs to the technical field of synthesis of
flame retardants. Tri (2-ethoxyl) isocyanurate,
phosphorus oxychloride and an
alcohol compound are used as raw materials, the cyan
phosphate is prepared through three-step reaction of preparing
phosphoryl chloride diester, refining the
phosphoryl chloride diester and synthesizing the cyan
phosphate, the molecular structure contains a
phosphate group and a
triazine ring conjugated structure, and a
carbon source, a gas source and an acid source are integrated. The
thermal decomposition temperature of the sec phosphate is greater than or equal to 320 DEG C, the UL94V-0 level
flame retardant standard can be reached by adding 12%-15% of sec phosphate into a
high polymer material, and the sec phosphate has the characteristics of high
flame retardant efficiency, good compatibility, strong migration resistance, excellent
thermal stability,
environmental protection and
low toxicity; the synthetic preparation method is stable in process, easy in condition control and high in product purity, can be widely applied to flame-retardant modification of
high polymer materials such as
polyvinyl chloride,
polyurethane and
epoxy resin, and has important industrial application value.