Preparation method of LED cold light solidified ink binder
A linking material and luminescent technology, applied in ink, household utensils, applications, etc., can solve the problems of difficult cleaning and disinfection, large loss, energy consumption, etc., and achieve excellent flexibility, abrasion resistance, and good durability.
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Embodiment 1
[0018] raw material A
[0019] TDI 0.5moL,
[0020] HDI 0.5moL;
[0021] raw material B
[0022]
[0023] raw material C
[0024] Polytetrahydrofuran 0.15moL;
[0025] The preparation method is as follows:
[0026] Put the raw material A and the catalyst (organotin, the addition amount is 0.1-3% of the total feeding amount) into the kettle, start the stirring, and let in dry nitrogen. The mixture of raw material B and raw material C is added dropwise, and the reaction is kept at 40-75°C for 1.5-5 hours until the NCO reaction is complete and the reaction ends, and the resin of the present invention is obtained.
Embodiment 2
[0028] raw material A
[0029] TDI 0.3moL,
[0030] HDI 0.3moL,
[0031] IPDI 0.2moL,
[0032] MDI 0.2moL,
[0033] raw material B
[0034]
[0035] raw material C
[0036] Polytetramethylene ether glycol 0.2moL;
[0037] The preparation method is as follows:
[0038] Put the raw material A and the catalyst (organotin, the addition amount is 0.1-0.3% of the total feeding amount) into the kettle, start stirring, feed dry nitrogen, and drop the mixture of raw material B and raw material C. Insulate and react at 40-75° C. for 1.5-5 hours until the NCO reaction is complete and the end point of the reaction is obtained to obtain the resin of the present invention.
Embodiment 3
[0040] raw material A
[0041] IPDI 0.5moL,
[0042] MDI 0.5moL,
[0043] raw material B
[0044]
[0045] raw material C
[0046] Polytetrahydrofuran 0.2moL,
[0047] Polytetramethylene ether glycol 0.4moL;
[0048] The preparation method is as follows:
[0049] Put the raw material A and the catalyst (organotin, the addition amount is 0.1-0.3% of the total feeding amount) into the kettle, start stirring, feed dry nitrogen, and add the mixture of raw material A and raw material C dropwise. Insulate and react at 40-75° C. for 1.5-5 hours until the NCO reaction is complete and the end point of the reaction is obtained to obtain the resin of the present invention.
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