Forecasting method of wettability of low-melting-point element regulation and control silver solder

A prediction method and low melting point technology, applied in analyzing materials, measuring devices, material analysis using wave/particle radiation, etc., can solve problems such as high cost, low test efficiency, low efficiency, etc. The effect of reducing test workload and improving work efficiency

Active Publication Date: 2018-01-09
NORTH CHINA UNIV OF WATER RESOURCES & ELECTRIC POWER
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Chinese patent 201310040275.3 discloses a method for improving the wettability of solder by combining ultrasonic field and electrostatic field. This patent adopts the process of wetting test, sample photographing, and drawing software calibration to analyze the wetting angle and wetting area, and judge the brazing area. material wettability; although the ultrasonic + electrostatic composite field can effectively improve the solder wettability, but after a large number of wetting tests, sample photographs, and software calibration procedures to determine whether the wettability is good or bad, the process is complicated, the test cost is high, and the efficiency is high. low
The published Chinese patent 201510865787.2 uses an L-shaped or V-shaped base metal plate to test the wettability of the solder by the crawling area or distance (height) of the solder on both sides of the L-shaped or V-shaped base metal, but it needs to be fabricated L-shaped or V-shaped base metal, adding flux, wet heat preservation-cooling, area or distance measurement and other steps, the process procedure is quite complicated, the cost is high, and the test efficiency is very low
Patent CN201410707428.X discloses a method for calculating the wetting speed of Sn-based solder and Cu substrate. The formula of wetting speed is established by means of the relationship between the area of ​​the wetting spot, the effective radius of the wetting spot, and time, but the image acquisition , Establish time-wetting spot area relationship curve, time-wetting spot effective radius relationship curve, the test workload is huge, the accuracy rate is poor, and the calculation efficiency is low

Method used

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  • Forecasting method of wettability of low-melting-point element regulation and control silver solder
  • Forecasting method of wettability of low-melting-point element regulation and control silver solder
  • Forecasting method of wettability of low-melting-point element regulation and control silver solder

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Experimental program
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Effect test

Embodiment 1

[0023] Embodiment 1: a method for predicting wettability of silver solder (AgCuZnSn, Sn content no more than 6.5%) in stainless steel surface controlled by Sn element, it comprises the following steps:

[0024] Step 1: adopt XRF-1800 type X-ray fluorescence spectrometer (XRF) to measure the content W of Sn element in solder M % (mass fraction);

[0025] Step 2: Use the STA449F3 thermal analyzer (DSC) to determine the solder melting temperature range ΔT M ;

[0026] Step 3: The content W of the different low melting point elements in the first step M % Expand 100 times and the melting temperature interval data ΔT of step 2 M Substitute into the forecasting mathematical model S M .

[0027]

[0028] Since it contains a low melting point element, n=1.

[0029] Step 4: According to Step 3 S M The size of the value determines the influence of Sn element on the wettability of the solder. The larger the value, the better the wettability of the solder, otherwise the worse th...

Embodiment 2

[0033] Embodiment 2: A method for predicting wettability of silver solder (AgCuZnIn, In content not exceeding 5.5%) regulated by In element on the surface of 316 stainless steel, the steps of which are the same as in Embodiment 1.

[0034] The specific data are shown in Table 2 below:

[0035]

[0036] According to Table 2, with the increase of In content, the S of AgCuZnIn solder on the surface of 316 stainless steel M The value gradually increases, indicating that its wettability is getting better and better; the test results show that with the increase of In content, the solder wetting area gradually increases.

[0037] The test results are consistent with the predicted results of the present invention.

Embodiment 3

[0038] Embodiment 3: A method for predicting wettability of silver solder (AgCuZnGa, Ga content less than 6.5%) regulated by Ga element on the surface of H62 brass, the steps of which are the same as in Embodiment 1.

[0039] The specific prediction data and test results are shown in Table 3 below:

[0040]

[0041] According to Table 3, with the increase of Ga content, the S of AgCuZnGa solder on the surface of H62 brass M The value gradually increases, indicating that its wettability is getting better and better; the test results show that with the increase of Ga content, the solder wetting area gradually increases. The test results are consistent with the predicted results of the present invention.

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Abstract

The invention discloses a forecasting method of wettability of a low-melting-point element regulation and control silver solder. The forecasting method comprises the following steps: 1, measuring thecontent WM% (mass percent) of each low-melting-point element in the silver solder; 2, determining a melting temperature range delta TM of the silver solder; 3, expanding the contents WM% of differentlow-melting-point elements in the step 1 for 100 times, and respectively substituting the expanded contents and the melting temperature range data delta TM in the step 2 into a built forecasting mathematical model SM; 4, judging the wettability of the silver solder according to an SM value in the step 3, wherein a larger value indicates higher wettability of the silver solder, and then otherwise,a smaller value indicates lower wettability. By combination of the melting temperature region of the low-melting-point-element-containing solder, the contents of the low-melting-point elements and theforecasting mathematical model, the forecasting method can quickly, efficiently and accurately forecast the wettability of the low-melting-point element regulation and control silver solder.

Description

Technical field: [0001] The invention belongs to the field of brazing filler metal performance evaluation, and in particular relates to a prediction method for adjusting and controlling the wettability of silver brazing filler metal by low-melting point elements. Background technique: [0002] As an important index to evaluate the performance of solder, wettability directly affects the filling ability of solder and the quality and performance of brazed joints, which in turn affects the service life and reliability of the parts to be brazed. Therefore, solder wettability is one of the key scientific issues in the study of brazing materials. [0003] Low-melting-point elements (melting point lower than 350°C) have the beneficial effect of reducing the melting temperature of the solder and improving the wettability of the solder. For silver solder with moderate melting temperature and excellent gap-filling ability, a certain amount of low-melting point is added Elements can ef...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N23/223B23K31/12
Inventor 王星星崔大田薛鹏彭进孙国元
Owner NORTH CHINA UNIV OF WATER RESOURCES & ELECTRIC POWER
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