The invention discloses a preparation method for producing an ultra-
pure oxygen-free
copper rod through an up-drawing
continuous casting method, and belongs to the technical field of
metal material
machining. Comprising the following steps: selecting a
cathode copper sheet as a
raw material, performing
oxygen-free
copper rod traction in a three-body furnace consisting of a
melting furnace, a transition bin and a holding furnace by adopting an up-drawing
continuous casting method, adding the dried electrolytic copper sheet and
charcoal into the
melting furnace, and adjusting the temperature of a melt in the
melting furnace; the molten copper liquid automatically flows into a transition bin to be subjected to standing and
impurity removal, and
charcoal and
graphite flakes are laid on the surface of the copper liquid; a
graphite crystallizer is inserted into molten copper, a guide rod is connected, a guide rod is prepared, the inlet and outlet
water temperature of the crystallizer is adjusted, and the traction speed and
pitch of a cast rod are set. According to the method, the
oxygen content of the produced ultra-
pure oxygen-free copper rod can be reduced to 3 ppm or below by controlling the quality of the
cathode copper sheet of the copper rod, the temperature of the copper liquid, the solidification
supercooling degree of the copper rod, the rod
casting speed, the conditions of the crystallizer and combined control over
charcoal and
graphite flake reduction, and the application additional value of the
oxygen-free copper rod is greatly improved.