Battery leakage detection method

A battery, leak detection technology, applied in the direction of detecting the appearance of fluid at the leak point, using liquid/vacuum degree for liquid tightness measurement, etc., can solve the problems of high price, low detection efficiency, high equipment and environmental requirements

Inactive Publication Date: 2018-04-03
HUNAN LIFANG NEW ENERGY SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Patent CN201520158858 provides a positive and negative pressure leak detection method, suitable for leak detection of batch batteries, suitable for batteries with serious leakage, and low detection efficiency for batteries with subtle defects
In addition, helium detection methods have appeared in recent years, such as patents CN201320619362 and CN201710125397. This method has the characteristics of high detection rate, but this method has high requirements on equipment and environment, is expensive, and has low detection efficiency.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] This embodiment provides a battery leak detection method, including the following steps:

[0026] Step 1, the electrolyte and the tracer are added to the battery in sequence, and the packaging of the battery is completed;

[0027] Step 2, place the battery obtained in Step 1 in a closed container equipped with a mass spectrometer, evacuate the container to a vacuum degree of -20Kpa, keep the pressure for 120s, and then fill it with air, and cycle 2 times like this;

[0028] Step 3, turn on the mass spectrometer, detect the gas extracted from the airtight container, and judge whether the cell leaks according to whether the tracer is detected;

[0029] where the tracer is the containing element 15 N substances, and the tracer does not corrode the pole pieces, current collectors, tabs and packaging materials, and does not react with the electrolyte or have no negative reactions that affect the performance of the electrolyte.

Embodiment 2

[0031] This embodiment provides a battery leak detection method, including the following steps:

[0032] Step 1, the electrolyte and the tracer are mixed first, and then injected into the battery together, and the packaging of the battery is completed;

[0033] Step 2, place the battery obtained in Step 1 in a closed container equipped with a mass spectrometer, evacuate the container to a vacuum degree of -40Kpa, and keep the pressure for 100s, then fill it with nitrogen, and cycle 2 times like this;

[0034] Step 3, turn on the mass spectrometer, detect the gas extracted from the airtight container, and judge whether the cell leaks according to whether the tracer is detected;

[0035] where the tracer is the containing element 13 Substance C, and the tracer does not corrode the pole pieces, current collectors, tabs and packaging materials, and does not react with the electrolyte or have no negative reactions that affect the performance of the electrolyte.

Embodiment 3

[0037] This embodiment provides a battery leak detection method, including the following steps:

[0038] Step 1, the electrolyte and the tracer are mixed first, and then injected into the battery together, and the packaging of the battery is completed;

[0039] Step 2, place the battery obtained in Step 1 in a closed container equipped with a mass spectrometer, evacuate the container to a vacuum degree of -60Kpa, keep the pressure for 80s, and then fill it with argon, and cycle 3 times like this;

[0040] Step 3, turn on the mass spectrometer, detect the gas extracted from the airtight container, and judge whether the cell leaks according to whether the tracer is detected;

[0041] where the tracer is the containing element 2 H substances, and the tracer does not corrode the pole pieces, current collectors, tabs and packaging materials, does not react with the electrolyte or has no negative reactions that affect the performance of the electrolyte.

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PUM

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Abstract

The invention provides a battery leakage detection method. The method includes following steps: step 1, injecting electrolyte and a tracer agent into a battery, and completing encapsulation of the battery; step 2, putting the battery obtained in the S1 into a closed container with a mass spectrometer, vacuumizing the container, holding pressure, filling gas, and repeating in this way; step 3, starting the mass spectrometer, detecting gas extracted from the closed container, and judging whether the battery leaks or not according to whether the tracer agent is present or not, wherein the traceragent is a substance containing at least one of elements 15N, 13C, 14C, 17O, 18O, 2H and 3H, does not corrode pole pieces, current collectors, pole lugs and an encapsulation material and does not react with the electrolyte or is not in negative reaction affecting performance of the electrolyte. By the method, defective batteries can be screened out conveniently and quickly to avoid potential safety hazards caused by the fact that the defective batteries having risk of electrolyte leakage go to clients.

Description

technical field [0001] The invention belongs to the technical field of batteries, and in particular relates to a battery leak detection method. Background technique [0002] In the process of secondary battery manufacturing, the following conditions may cause battery leakage: 1) Insufficient battery circulation protection will cause defects such as battery surface damage and pinholes; 2) Battery packaging is incomplete due to equipment and personnel factors , there are leak seals, unpackaged, etc.; 3) The battery has leakage channels due to process problems. It should be noted that, on the one hand, electrolyte leakage will cause battery performance to decline; on the other hand, it will cause terminal corrosion, and defective channels will cause safety hazards, such as LiPF 6 The electrolyte absorbs water through defective channels, causing the battery to gas. [0003] In order to avoid the impact of electrolyte leakage on the electrochemical performance and safety perfor...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01M3/20
Inventor 朱登伟
Owner HUNAN LIFANG NEW ENERGY SCI & TECH
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