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A batching method for uhmwpe fiber production that realizes continuous and uniform feeding

A uniform and feeding technology, applied in fiber processing, fiber chemical characteristics, textiles and papermaking, etc., can solve the problems that the concentration gradient of UHMWPE powder cannot be completely eliminated, the feeding pipeline of the reactor cannot be stirred, and the molecular conformation of the product denier is affected. , to achieve the effect of automatic continuous and uniform feeding, improved thermal conductivity and creep resistance, and improved conveying capacity

Active Publication Date: 2020-04-24
龙游龙纤新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This batching method not only has a large deviation between batches, but also has a density difference between white oil and UHMWPE powder. The concentration gradient in the vertical direction, and there is a dead angle in the reactor, and the stirring cannot be realized inside the feeding pipe, so the difference in ingredients is more significant
This difference is reflected in the production, the melt viscosity and the head pressure fluctuate periodically, and the deviation can reach 10%, which in turn affects the product fineness and the molecular conformation of UHMWPE, and finally leads to the performance of the product

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] 1) Prepare a uniform solution with a concentration of 0.1-1% UHMWPE / white oil; put the UHMWPE powder, polyolefin antioxidant and white oil into the reaction kettle to accurately measure polyolefin antioxidant, UHMWPE and white oil, The mass of polyolefin antioxidant accounts for 5% to 10% of the mass of UHMWPE powder;

[0025] Gradually raise the temperature to 140°C under stirring, stir for 10-30 minutes, continue to raise the temperature to 160°C, stir for 10-30 minutes, and continue to raise the temperature to 180°C. There will be a significant pole climbing effect during the UHMWPE dissolution process, and the stirring speed can be appropriately reduced according to the production situation when the pole climbing effect occurs. After the temperature reaches 180°C, continue to keep stirring for 30 minutes. Add a certain amount of cold white oil to lower the temperature of UHMWPE / white oil to below 120°C, and set it aside. Dilute the ready-to-use UHMWPE / white oil so...

Embodiment 2

[0035] Utilize the working curve of the loss-in-weight scale to calculate the difference between the actual feeding speed and the set value in Example 1, and calculate the batching error; the result proves that the batching error is <0.1%.

[0036] By detecting the online viscosity change of the screw discharge, because the feeding deviation is proportional to the screw discharge viscosity change, the melt viscosity change is tested for a period of time, and the result proves that the batching accuracy is increased from 1.2% to 0.097%.

[0037] Adopt the batching mode that embodiment 1 obtains, (1) the precision of batching is higher, and uneven rate is less than 0.1%, has reduced the impact of uneven batching on product quality; (2) by improving the consistency of product, has improved product performance ;(3) Add various inorganic particles to realize different functions of UHMWPE fibers, as shown in Table 1 above; (4) Compared with kettle-type ingredients, switching product ...

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Abstract

The invention provides a new UHMWPE fiber production batching method capable of achieving continuous and uniform feeding. The method includes the following steps that 1, UHMWP solution with the concentration of 0.1-1% is prepared; 2, an ingredient is put into a strong shear dispersing device and shorn and dispersed to be uniform and stable; 3, UHMWPE powder, the UHMWP solution prepared in the step1 and the ingredient obtained in the step 2 are metered through a weightlessness scale and fed, wherein the weightlessness scale is provided with an automatic material supplementing device. By adopting the weightlessness scale for vector control, feeding is automatic, continuous and uniform, the batching error is smaller than 0.1%, the batching accuracy is improved to 0.097% from 1.2%, under thesame production conditions, the fineness CV value of UHMWPE fiber is reduced to 0.52% from 3.1%, the hyperploids stretch ratio of the fiber is increased by 3-10%, and strength, modulus, abrasion resistance, heat conductivity and creep resistance of the fiber are improved; the product strength is smaller than 42 g / d, and the modulus is smaller than 1650 g / d.

Description

technical field [0001] The invention belongs to the field of UHMWPE fiber production, and in particular relates to a method for producing ingredients for UHMWPE fiber that realizes continuous and uniform feeding. Background technique [0002] UHMWPE (Ultra High Molecular Weight Polyethylene) is a thermoplastic engineering plastic with a linear structure and excellent comprehensive properties, with a molecular weight of more than 1.5 million. UHMWPE fiber is a flexible chain polymer with high strength and high modulus, and its molecular microstructure is extremely regular. Because of its inert chemical structure, and highly oriented and highly crystalline structure, it has excellent performance in both chemical and physical properties, and has mechanical properties unmatched by other high-performance fibers. The third generation of high-performance fibers after aramid. Low density, good wear resistance, self-lubrication, impact resistance, corrosion resistance and so on. ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01D1/00D01F6/46D01F1/10
CPCD01D1/00D01F1/10D01F6/46
Inventor 姚湘江陈宏
Owner 龙游龙纤新材料有限公司
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