A batching method for uhmwpe fiber production that realizes continuous and uniform feeding
A uniform and feeding technology, applied in fiber processing, fiber chemical characteristics, textiles and papermaking, etc., can solve the problems that the concentration gradient of UHMWPE powder cannot be completely eliminated, the feeding pipeline of the reactor cannot be stirred, and the molecular conformation of the product denier is affected. , to achieve the effect of automatic continuous and uniform feeding, improved thermal conductivity and creep resistance, and improved conveying capacity
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Embodiment 1
[0024] 1) Prepare a uniform solution with a concentration of 0.1-1% UHMWPE / white oil; put the UHMWPE powder, polyolefin antioxidant and white oil into the reaction kettle to accurately measure polyolefin antioxidant, UHMWPE and white oil, The mass of polyolefin antioxidant accounts for 5% to 10% of the mass of UHMWPE powder;
[0025] Gradually raise the temperature to 140°C under stirring, stir for 10-30 minutes, continue to raise the temperature to 160°C, stir for 10-30 minutes, and continue to raise the temperature to 180°C. There will be a significant pole climbing effect during the UHMWPE dissolution process, and the stirring speed can be appropriately reduced according to the production situation when the pole climbing effect occurs. After the temperature reaches 180°C, continue to keep stirring for 30 minutes. Add a certain amount of cold white oil to lower the temperature of UHMWPE / white oil to below 120°C, and set it aside. Dilute the ready-to-use UHMWPE / white oil so...
Embodiment 2
[0035] Utilize the working curve of the loss-in-weight scale to calculate the difference between the actual feeding speed and the set value in Example 1, and calculate the batching error; the result proves that the batching error is <0.1%.
[0036] By detecting the online viscosity change of the screw discharge, because the feeding deviation is proportional to the screw discharge viscosity change, the melt viscosity change is tested for a period of time, and the result proves that the batching accuracy is increased from 1.2% to 0.097%.
[0037] Adopt the batching mode that embodiment 1 obtains, (1) the precision of batching is higher, and uneven rate is less than 0.1%, has reduced the impact of uneven batching on product quality; (2) by improving the consistency of product, has improved product performance ;(3) Add various inorganic particles to realize different functions of UHMWPE fibers, as shown in Table 1 above; (4) Compared with kettle-type ingredients, switching product ...
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