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749results about "Filament-forming treatment" patented technology

Method for continuous production of polyamide

Provided is a continuous production method of a polyamide with stabilized polymerization degree and good quality, particularly an aromatic-containing polyamide. A continuous production method of a polyamide, comprising (a) a raw material preparation step of individually melting a diamine and a dicarboxylic acid, or producing a salt of amine and carboxylic acid in water, (b) a raw material introduction step of continuously introducing the prepared raw materials into a tubular reaction apparatus, (c) an amidation step of passing the introduced raw materials through the tubular reaction apparatus, thereby effecting amidation to obtain a reaction mixture containing an amidated product and a condensed water, (d) an initial polymerization step of introducing the reaction mixture into a continuous reaction apparatus capable of separation and removal of water, and elevating the polymerization degree while separating and removing water at a temperature higher than the melting point of the finally obtained polyamide to obtain a polyamide prepolymer, and (e) a final polymerization step of introducing the polyamide prepolymer into a continuous reaction apparatus capable of separation and removal of water, and further elevating the polymerization degree at a temperature higher than the melting point of the finally obtained polyamide to obtain a polyamide adjusted to a desired relative viscosity [RV].
Owner:TOYOBO CO LTD

Production method of fine-denier porous POY black yarn

The invention discloses a production method of a fine-denier porous POY black yarn. The method comprises the following steps of: drying semi-dull slices, drying black masterbatch, adding the slices and the black masterbatch material into a screw extruder, fusing the added materials in the screw extruder, respectively processing the fused materials in a metering pump and a spinning beam, spinning on a pack, cooling the materials by lateral blowing, applying oil on strands, processing the strands in draw-off godets GR1 and GR2, winding and shaping, and inspecting products. The method is characterized in that the step of drying the black masterbatch comprises the following sub-steps of: based on a continuous drying mode, firstly, adding the black masterbatch into a crystallization and drying tank, introducing heated dry air from the lower part of the crystallization and drying tank, and blowing out the heated dry air from the top of the crystallization and drying tank so as to dry the black masterbatch, wherein the drying time is 2 hours, the dried black masterbatch falls into an intermediate material storage bin for storage under the crystallization and drying tank, and the black masterbatch is further injected by a masterbatch injector under the intermediate material storage bin. The production method of the fine-denier porous POY black yarn has high masterbatch spinnability and better cooling effect, and can improve the oil application uniformity of spinning cakes and the productivity.
Owner:桐乡市中洲化纤有限责任公司

Method for preparing colorized fire-retardant delustering hollow polyester filament

The invention relates to a method for preparing a polyester filament, in particular to a method for preparing a colorized fire-retardant delustering hollow polyester filament. The method mainly solves the technical problem of the prior art that color master batches and a delustering agent added into a fire-retardant slice can influence the viscosity of a fused mass during the spinning and the friction to a device in the processing process so that colorized, fire-retardant and delustering finished polyester fiber and the like cannot be prepared. The preparation method comprises the following steps: adding a copolymerization fire retardant in the process of preparing a polyester slice to form the fire-retardant slice; performing pre-crystallization on and drying the fire-retardant slice, the color master batches and delustering master batches, and evaporating the water content; mixing the fire-retardant slice with the color master batches and the delustering master batches, passing the mixture into a double screw extruder to perform heating melting, performing filter mixing and measuring allocation on the fused mass, and spinning the fused mass into tows; and performing cooling molding on the tows through lateral blow, and obtaining a finished product after oil tanker oiling, drafting, networking and winding.
Owner:ZHEJIANG HUAXIN ADVANCED MATERIALS

Elastic nonwoven fabric, process for producing the same, and textile product comprising the elastic nonwoven fabric

(1) An elastic nonwoven fabric and a fiber product using the elastic nonwoven fabric, the elastic nonwoven fabric containing a crystalline resin composition containing low crystalline polypropylene and high crystalline polypropylene, the low crystalline polypropylene satisfying items (a) and (b) below, and a crystallization temperature (Tc) of the crystalline resin composition measured with a differential scanning calorimeter (DSC) being from 20 to 100° C.:
(a) a melting point (Tm-D) being from 0 to 120° C., which is defined as a peak top of a peak observed on the most high temperature side of a melt endothermic curve obtained by maintaining at −10° C. for 5 minutes and increasing in temperature at 10° C. per minute in a nitrogen atmosphere with a differential scanning calorimeter (DSC); and
(b) a stereoregularity index ([mm]) being from 50 to 90% by mol;
(2) an elastic nonwoven fabric and a fiber product using the elastic nonwoven fabric, the elastic nonwoven fabric being produced by using a crystalline resin composition containing low crystalline polypropylene satisfying items (c) to (h) below, and a releasing agent: (c) [mmmm]=20 to 60% by mol; (d) [rrrr]/(1−[mmmm])≦0.1; (e) [rmrm]>2.5% by mol; (f) [mm]×[rr]/[mr]2≦2.0; (g) mass average molecular weight (Mw)=10,000 to 200,000; and (h) molecular weight distribution (Mw/Mn)<4; and
(3) an elastic nonwoven fabric and a fiber product using the elastic nonwoven fabric, the elastic nonwoven fabric containing core/shell type composite fibers containing low crystalline polypropylene satisfying the items (c) to (h) have excellent elastic recovery property and pleasant texture without stickiness.
Owner:IDEMITSU KOSAN CO LTD

Method for preparing polyimide fibers

The invention discloses a method for preparing polyimide fibers, and belongs to the technical field of the polyimide fibers. The method is characterized in that: polyamide acidic solution is subjected to spinning by adopting a wet spinning or dry wet spinning process, and fibers are subjected to processes of coagulating and drying or processes of washing, drying, heat treatment cyclizing and stretching continuously and are rolled finally to form the polyimide fibers. The method comprises the following specific steps of: reacting diamine with dianhydride in solvent under the protection of nitrogen to obtain polyamide acidic spinning solution; filtering the spinning solution, pouring the filtered spinning solution into a storage tank for defoaming, spinning according to the wet spinning or dry wet spinning process, pumping the spinning solution by a metering pump, and spraying from a spinneret plate; dragging by a silk guide roller, coagulating in coagulating bath, drying directly by a hot roller or a hot plate or drying by the hot roller or the hot plate after washing, and performing heat cyclizing and stretching by three sections or more than three sections of furnace sections; and finally, rolling silk. In the method, the integral process is continuous, smooth, compact and short in time, high imidization degree and degree of orientation are realized, and the high-performance fibers are obtained.
Owner:JIANGSU XIANNUO NEW MATERIAL TECH

Preparation method for super fine denier polyester filaments

The invention relates to the technical field of preparation methods for polyester filaments, particularly to a preparation method for super fine denier polyester filaments. The preparation method adopts super bright PET chips as raw materials to implement the production through the steps of pre-crystallization, drying, extrusion, filtering, distribution of spinning box bodies, filament splitting by a metering pump, filament spraying, lateral air blowing, winding and packing of finished products. According to the preparation method adopted by the invention, finally finished fibers have the performances of high strength, low elongation, low heat shrinkage and the like; the breaking strength of the fibers is larger than 7.0 cN/dtex; the breaking elongation of the fibers is less than 14%; the boiling water shrinkage of the fibers is less than 1.8%; and the dry heat shrinkage is less than 4.5%. And at the same time, the preparation method has the characteristics of short production flow, high spinning speed, fewer broken filaments, fewer broken ends, low production cost and the like, and is not only used for top grade sewing threads, embroidery threads and fishing nets, but also heavily applied in various vehicle airbags, base camp tent fabrics and various industries adopting high strength fibers as auxiliary materials or reinforcing materials.
Owner:NANTONG HUALUN CHEM FIBER

Polyester elastomer/PET composite elastic fiber and preparation method thereof

The invention discloses a polyester elastomer / PET composite elastic fiber and a preparation method thereof. The preparation method comprises the steps of firstly carrying out reduced-pressure direct esterification on terephthalic acid, 1,4-butanediol and double-ended hydroxyl polyether in a certain proportion in the presence of catalysts, carrying out melt polycondensation to obtain a polyester elastomer, and carrying out a spin-draw-winding one-step process on the prepared polyester elastomer and PET, so as to obtain the polyester elastomer / PET composite elastic fiber, wherein the breaking strength of the polyester elastomer / PET composite elastic fiber is 2.8cN / dtex-3.56cN / dtex, the elongation at break is 16.9%-30.4%, the curling degree is 60%-75%, the curling elasticity rate is 97%-99%, the capillary water absorption height is 9.7cm / 30min-14.1cm / 30min. Compared with normal composite elastic fibers, the polyester elastomer / PET composite elastic fiber has relatively excellent elasticity and relatively soft hand feeling, and the fabric capillary suction effect of the polyester elastomer / PET composite elastic fiber is even higher than those of cotton fabrics; the preparation method is short in production process, high in spinning speed and low in cost, and the prepared composite elastic fiber can be directly used in subsequent weaving without being processed into interlaced yarns.
Owner:SICHUAN UNIV +1

Cellulose dip cord produced from highly homogeneous cellulose solution and tire using the same

The present invention relates to a method for producing tire using high strength lyocell dip cord, and more particularity, to a lyocell dip cord and tire produced by a method comprising the steps of: (A) dissolving 0.01 to 3 wt % of cellulose powder in portions in concentrated liquid N-methylmorpholine N-oxide (NMMO) to prepare cellulose-containing NMMO solution; (B) feeding the NMMO solution and cellulose powder into an extruder having a screw to be subjected to dispersing, mixing, shearing, kneading, melting and measuring ability in the extruder to prepare a swollen and homogenized cellulose solution; (C) spinning the cellulose solution through a spinning nozzle, passing the spinning solution through an air gap to a coagulation bath and coagulating the spinning solution to obtain a multifilament; (D) subject the multifilament to water-wash, drying and oil-treatment, followed by winding; and (E) twisting the wound yarn with a twisting machine to prepare a greige cord, weaving the greige cord and dipping the woven cord in a dipping solution. According to the present invention, by lowering of solidification temperature of NMMO by dissolving a small amount of pulp in concentrated liquid NMMO, it is possible to prepare a homogeneous cellulose solution at a low temperature. Also, the lyocell dip cord prepared according to the present invention has excellent adhesion to rubber, tenacity and modulus. And, the tire in which the lyocell dip cord according to the present invention is applied to the carcass ply has excellent dimensional stability and handling stability.
Owner:HYOSUNG ADVANCED MATERIALS CORP

Method for continuous production of polyamide

Provided is a continuous production method of a polyamide with stabilized polymerization degree and good quality, particularly an aromatic-containing polyamide. A continuous production method of a polyamide, comprising (a) a raw material preparation step of individually melting a diamine and a dicarboxylic acid, or producing a salt of amine and carboxylic acid in water, (b) a raw material introduction step of continuously introducing the prepared raw materials into a tubular reaction apparatus, (c) an amidation step of passing the introduced raw materials through the tubular reaction apparatus, thereby effecting amidation to obtain a reaction mixture containing an amidated product and a condensed water, (d) an initial polymerization step of introducing the reaction mixture into a continuous reaction apparatus capable of separation and removal of water, and elevating the polymerization degree while separating and removing water at a temperature higher than the melting point of the finally obtained polyamide to obtain a polyamide prepolymer, and (e) a final polymerization step of introducing the polyamide prepolymer into a continuous reaction apparatus capable of separation and removal of water, and further elevating the polymerization degree at a temperature higher than the melting point of the finally obtained polyamide to obtain a polyamide adjusted to a desired relative viscosity [RV].
Owner:TOYO TOYOBO CO LTD

Easy-to-dye terylene BCF and method for preparing same

InactiveCN101338455AImprove spinnabilitySolve the two major problems of dyeing at room temperatureFibre mixingLap-winding devicesFiberYarn
The invention relates to a chromophil terylene BCF and a preparation method thereof, which belong to the technical field of the terylene. The chromophil terylene BCF is characterized in that the terylene BCY is in a tri-leaflet shape which is also called as Y-shaped microcellular structure. The preparation method is characterized in that (1) the slice of raw terylene materials is pre-crystallized and dried by a dryer; (2) the slice of the raw terylene materials are melted by an extruder; (3) multifilament yarn which is in the tri-leaflet shape which is also called as the Y-shaped microcellular structure is sprayed by a tri-leaflet spinneret plate; (4) a tow is cooled to be formed into initial raw silk; (5) oil solution is applied to spinning; (6) the spinning is extended; (7) the spinning undergoes the process of bulking in a deformation box; (8) the spinning is cooled and curled; (9) the spinning undergoes the process of link making; (10) the spinning is rolled into a drum. The chromophil terylene BCF solves two problems that the current BCF has poor spinnability and is difficult to be dyed under normal temperature, provides newly-invented BCF fiber for manufacturing the suede of a blanket and creates conditions for manufacturing the blanket that has good spreadability, beautiful appearance and low manufacturing cost.
Owner:上海繁太实业有限公司
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