A kind of fine denier snow lotus microcapsule cellulose fiber and its preparation method

A cellulose fiber and microcapsule technology, which is applied in the directions of microcapsule preparation, microsphere preparation, cellulose/protein conjugated artificial filament, etc. Cellulose fibers, insufficient softness and comfort, etc., to achieve the effects of low preparation fineness, improved embedding rate and sphericity, and good skin care

Active Publication Date: 2020-09-11
ZHONGKE TEXTILE RES INST QINGDAO CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, adding Saussurea oleracea extract components to viscose fibers provides a fiber with good freckle removal, beauty treatment, and antibacterial effects and is applied to skin care products without any reports. On the whole, the prior art has the following defects:
[0003] 1. In the prior art, there is no report on the cellulose fiber prepared by combining the beauty and whitening, tissue repair, freckle removal, antibacterial, anti-inflammatory and silk fibroin of snow lotus;
[0004] 2. Due to the fiber fineness of conventional cellulose fibers, the skin care and health care products made of conventional cellulose fibers are not soft enough, and the fit with the face is not enough, which brings discomfort and irritation to the skin and face. ;
[0005] 3. In the process of preparing functional fibers by conventional methods, microcapsules are often used to reduce the loss of additives. However, the particle size of microcapsules prepared by conventional methods is large, and adding them to fibers with small fineness will have a negative effect on the fibers. Therefore, the microcapsules prepared by conventional methods are not suitable for the preparation of fine denier cellulose fibers because of their large particle size

Method used

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  • A kind of fine denier snow lotus microcapsule cellulose fiber and its preparation method
  • A kind of fine denier snow lotus microcapsule cellulose fiber and its preparation method
  • A kind of fine denier snow lotus microcapsule cellulose fiber and its preparation method

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Experimental program
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Effect test

Embodiment 1

[0058] Embodiment 1 A kind of preparation method of fine denier snow lotus microcapsule cellulose fiber,

[0059] Include the following steps:

[0060] (1) Preparation of snow lotus extract emulsified dispersion

[0061] The content of the active ingredient is 18% peach gum solution, 10 parts of the purchased snow lotus extract and 15 parts of the peach gum solution are mixed, heated to 65 ° C, stirred and emulsified, and the stirring speed is 200 r / min, so that the snow lotus extract is emulsified Disperse, after being completely dissolved, filter, and remove insoluble impurities to obtain snow lotus extract emulsified dispersion;

[0062] Snow lotus extract, brown powder, 100% passed through 80 mesh sieve, ash content≤3.2%, moisture content≤3.8%, heavy metal content≤5ppm, lead content≤1ppm, arsenic content≤0.5 ppm, mercury content≤0.4 ppm, total bacteria ≤500cfu / g, the total number of molds ≤50 cfu / g, Salmonella and Escherichia coli shall not be detected.

[0063] (2) Pre...

Embodiment 2

[0083] Embodiment 2 A kind of preparation method of fine denier snow lotus microcapsule cellulose fiber,

[0084] Include the following steps:

[0085] (1) Preparation of snow lotus extract emulsified dispersion

[0086] Calculate the parts by weight of the snow lotus extract and the peach gum solution, mix 8 parts of the snow lotus extract and 17 parts of the peach gum solution, heat to 65 ° C after mixing, stir and emulsify, and the stirring speed is 220r / min, so that the snow lotus extract is emulsified and dispersed, After being completely dissolved, the insoluble impurities are removed by filtration to obtain a snow lotus extract emulsified dispersion;

[0087] The snow lotus extract is produced by Xi'an Virgin Biotechnology Co., Ltd. and is commercially available;

[0088] The peach gum solution is prepared by dissolving peach gum in water; the content of the active ingredient of peach gum in the peach gum solution is 18%;

[0089] The snow lotus extract, brown powder...

Embodiment 3

[0113] Embodiment 3 A kind of preparation method of fine denier snow lotus microcapsule cellulose fiber,

[0114] Include the following steps:

[0115] (1) Preparation of snow lotus extract emulsified dispersion

[0116] Calculate the parts by weight of the snow lotus extract and the peach gum solution, mix 8 parts of the snow lotus extract and 158 parts of the peach gum solution, heat to 870 ° C, stir and emulsify, and the stirring speed is 200r / min, so that the snow lotus extract is emulsified and dispersed, After being completely dissolved, the insoluble impurities are removed by filtration to obtain a snow lotus extract emulsified dispersion; the snow lotus extract is produced by Xi'an Virgin Biotechnology Co., Ltd. and is commercially available; the peach gum solution is prepared by dissolving peach gum in water. ; The content of the active ingredient of peach gum in the peach gum solution is 18-20%;

[0117] The snow lotus extract, brown powder, 100% passed through 80 ...

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Abstract

The invention provides a fine-denier saussurea involucrata microcapsule cellulose fiber with a fineness of <=0.9 dtex, a dry breaking strength of 3.8-4.5 cN / dtex, a wet breaking strength of 2.4 -2.8 cN / dtex and a dry elongation at break of 22.6-24.5%. The invention also provides a preparation method of the fine-denier saussurea involucrata microcapsule cellulose fiber. The preparation method includes a preparation step of an emulsion dispersion solution of saussurea involucrata extract, a preparation step of a saussurea involucrata extract-Arabic gum composite dispersion solution, a preparation step of a saussurea involucrata extract microcapsule, a preparation step of a saussurea involucrata extract microcapsule suspension, a preparation step of a spinning solution and a preparation stepof a saussurea involucrata extract microcapsule spinning solution. The health care skin care products such as facial masks and wet wipes prepared from the fine-denier saussurea involucrata cellulose fiber can beautify and whiten the skin, are soft and comfortable, and have good fit with the face and the like without stimulation.

Description

technical field [0001] The invention relates to the field of cellulose fiber preparation, in particular to a fine denier snow lotus microcapsule cellulose fiber and a preparation method thereof. Background technique [0002] As we all know, the natural snow lotus contains rhododendron, snow lotus lactone, snow lotus polysaccharide, etc. Its sun protection factor is as high as 22SPF, which is much higher than the domestic super-intensity ultraviolet radiation of 15SPF. Therefore, it can effectively protect the skin from ultraviolet rays. It has obvious inhibitory effect on the increase of lipid peroxides in liver and serum caused by toxins in the body, indicating that snow lotus has anti-inflammatory, tissue repair and anti-superoxide free radical effects, and has anti-physiological or non-physiological factors ( Such as disease) to induce long-term chronic progressive damage of free radicals has positive significance. This effect is manifested as health care and immune enha...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F8/02D01F8/16D01F1/10B01J13/02D01D5/06D01D1/02A61K8/9789A61K8/73A61K8/64A61K8/02A61Q19/10A61Q19/00A61Q19/02A61Q19/08A61Q17/00A61L15/46A61L15/40A61L15/42A61L15/32A61L15/28
CPCA61K8/0212A61K8/64A61K8/731A61K8/97A61L15/28A61L15/32A61L15/40A61L15/42A61L15/46A61L2300/30A61L2300/404A61L2400/04A61Q17/005A61Q19/00A61Q19/02A61Q19/08A61Q19/10B01J13/02D01D1/02D01D5/06D01F1/10D01F8/02D01F8/16C08L89/00C08L1/24
Inventor 黄效龙刘洁
Owner ZHONGKE TEXTILE RES INST QINGDAO CO LTD
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