Hard natural fiber/polypropylene rosewood-imitating building material and preparation method thereof

A technology of natural fiber and polypropylene, which is applied in the field of hard natural fiber/polypropylene imitation mahogany building materials and its preparation, can solve the problems of poor compatibility between wood powder or wood fiber and non-polar matrix, and is suitable for industrialization promotion, The effect is realistic and improves the effect of the compound fill effect

Inactive Publication Date: 2019-03-01
CHENDU NEW KELI CHEM SCI CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] Aiming at the technical problems such as poor compatibility between wood powder or wood fiber and non-polar matrix in the current imitation mahogany materials, the first technical problem to be solved by the present invention is to provide a preparation method of hard natural fiber / polypropylene imitation mahogany building materials

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] Example 1 Preparation of a hard natural fiber / polypropylene imitation mahogany building material

[0035] Follow these steps:

[0036]a. Grinding and dispersing imitation mahogany color paste and natural wood fiber under cooking conditions for 4 hours, suction filtering and drying at 190°C to obtain dyed wood fiber;

[0037] b. Dissolve acetic anhydride and acid catalyst in supercritical carbon dioxide, mix with dyed wood fiber under 13MPa pressure, wait for the reaction to be completed, release the pressure, then recycle carbon dioxide, separate out the precipitate to obtain non-polarized dyed wood fiber; , the weight ratio of acetic anhydride to dyed wood fiber is 3.5:1.

[0038] c. Disperse the obtained non-polarized dyed wood fiber in the non-polar dispersion medium organic solvent silicone oil. The distearyl propionate is mixed, then put into a kneader for kneading treatment, and then put into a flat vulcanizer for hot-press molding to obtain a hard imitation mah...

Embodiment 2

[0039] Example 2 Preparation of a hard natural fiber / polypropylene imitation mahogany building material

[0040] Follow these steps:

[0041] a. Grinding and dispersing imitation mahogany color paste and natural wood fiber under cooking conditions for 3 hours, suction filtering and drying at a drying temperature of 180°C to obtain dyed wood fiber;

[0042] b. Dissolve acetic anhydride and acid catalyst in supercritical carbon dioxide, mix with dyed wood fiber under 10MPa pressure, wait for the reaction to be completed, release the pressure, then recover carbon dioxide, separate out the precipitate to obtain non-polarized dyed wood fiber; , the weight ratio of acetic anhydride and dyed wood fiber is 2:1.

[0043] c. Disperse the obtained non-polarized dyed wood fiber in the non-polar dispersion medium organic solvent silicone oil. (2,4-di-tert-butylphenyl) esters are mixed, then put into a kneader for kneading treatment, and then put into a flat vulcanizer for hot-press moldi...

Embodiment 3

[0044] Example 3 Preparation of a hard natural fiber / polypropylene imitation mahogany building material

[0045] Follow these steps:

[0046] a. Grinding and dispersing imitation mahogany color paste and natural wood fiber under cooking conditions for 5 hours, suction filtering and drying at 200°C to obtain dyed wood fiber;

[0047] b. Dissolve acetic anhydride and acid catalyst in supercritical carbon dioxide, mix with dyed wood fiber under 15MPa pressure, wait for the reaction to be completed, release the pressure, then recover carbon dioxide, separate out the precipitate to obtain non-polarized dyed wood fiber; , the weight ratio of acetic anhydride and dyed wood fiber is 5:1.

[0048] c. Disperse the obtained non-polarized dyed wood fiber in the non-polar dispersion medium organic solvent silicone oil. (2,4-di-tert-butylphenyl) esters are mixed, then put into a kneader for kneading treatment, and then put into a flat vulcanizer for hot-press molding to obtain a hard imit...

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PUM

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Abstract

The invention relates to a hard natural fiber / polypropylene rosewood-imitating building material and a preparation method, and belongs to the field of preparation of natural fiber composite rosewood-imitating materials. The preparation method of the hard natural fiber / polypropylene rosewood-imitating building material comprises the following steps that redwood color-imitating paste and natural wood fibers are ground and dispersed under a cooking condition, and suction filtration and drying are carried out to obtain dyed wood fibers; acetic anhydride and a catalyst are dissolved in supercritical carbon dioxide, and then are mixed with the dyed wood fibers under the pressure of 10-15 MPa, pressure relief is carried out after the reaction is completed, carbon dioxide is recovered, and a precipitate is separated out to obtain non-polar dyed wood fibers; and the obtained non-polar dyed wood fibers are dispersed in a non-polar dispersion medium, and then are mixed with a polypropylene matrixand an antioxidant, then mixing is carried out, a mixture is taken out, and then the mixture is put into a flat vulcanizing machine for hot-pressing forming to obtain the hard rosewood-imitating building material. The comprehensive use quality of the rosewood-imitating product prepared by using the preparation method is effectively enhanced, a good use value is achieved, and the effect is more vivid.

Description

technical field [0001] The invention relates to a hard natural fiber / polypropylene imitation mahogany building material and a preparation method, belonging to the field of preparation of natural fiber composite imitation wood materials. Background technique [0002] Natural fiber composite wood-like materials are new wood-like materials made of natural plant fiber materials from agricultural and forestry waste, such as wood powder, rice husk, straw, etc., and plastics, collectively referred to as wood-plastic materials. [0003] As we all know, the chemical structure of plant fibers such as wood flour and rice husk powder contains a large number of highly polar hydroxyl groups, and each cellulose ring contains multiple -OH groups. Both polyethylene and polypropylene resins are non-polar. Although PVC resin contains chlorine atoms and has certain polarity, its polarity is much smaller than that of cellulose, so they are two mutually incompatible systems-- Cellulose is a typi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B27N3/04B27N3/12B27N3/00B27N1/00B27K5/02B27K5/00
CPCB27N3/04B27K5/001B27K5/02B27K2200/15B27N1/00B27N3/002B27N3/007B27N3/12
Inventor 陈庆昝航
Owner CHENDU NEW KELI CHEM SCI CO LTD
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