Compound for organic electroluminescent device and application thereof
A technology for electroluminescent devices and compounds, applied in the fields of organic chemistry, electro-solid devices, electrical components, etc., can solve problems affecting device stability, imbalance of electron and hole charge mobility, and changes in device conductivity, etc. The effect of carrier mobility
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[0031] Hereinafter, the organic electroluminescent compound of the present invention, its preparation method, and the preparation method and light-emitting properties of a light-emitting device comprising the compound are described in detail with reference to the following examples.
[0032] Various chemicals used in the present invention such as petroleum ether, ethyl acetate, tetrahydrofuran, dioxane, toluene, acetic acid, methylene chloride, DMF, methyl o-iodobenzoate, tetrakistriphenylphosphine palladium, 2- Various boric acids or boric acid esters, phenylhydrazine hydrochloride, 4-bromophenylhydrazine hydrochloride, etc. Chemical product market to buy.
[0033] Preparation of Synthetic Example 1 Intermediate M1
[0034]
[0035] Under the protection of nitrogen, in the 250 milliliter three-neck flask that condenser tube is housed, add 27.2 gram borates (0.1mol), 28.8 gram o-iodobenzoic acid methyl esters (0.11mol), 1.15 gram tetrakistriphenylphosphine palladium (1mmol...
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