A kind of low temperature ceramic metal composite bond for abrasive tool and preparation method thereof
A composite bond, ceramic bond technology, applied in metal processing equipment, grinding/polishing equipment, abrasives, etc., can solve the problems of not too ideal composite effect, poor physical and chemical compatibility, etc., to improve the wetting condition , performance improvement, uniform structure effect
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Embodiment 1
[0026] Its technical scheme is: low-temperature vitrified bond powder 92% (volume percentage), nickel-phosphorus alloy 8%.
[0027] The raw material of low temperature vitrified bond is: silicon dioxide (SiO 2 ) 48%, alumina (Al 2 o 3 ) 6%, sodium carbonate (Na 2 CO 3 ) 6%, lithium carbonate (Li 2 CO 3 ) 5%, zirconia (ZrO 2 ) 2%, clay (Hydrotalcite) 8%, boric acid (H 3 BO 3 ) 25%.
[0028] The raw material of electroless plating solution is: nickel sulfate (NiSO 4 ) 30g / L, sodium hypophosphite (NaH 2 PO 2 ) 25g / L, sodium citrate (Na 3 C 6 h 5 o 7 2H 2 O) 25g / L, thiourea (CH 4 N 2 S) 0.001g / L.
[0029] The sintering temperature is 680°C, the pressure is 2MPa, and the pressure is maintained for 3min. The low-temperature ceramic-metal bond prepared has a flexural strength of 120~140MPa and an impact strength of 2~3kJ / m 2 , hardness 120~122HRB.
Embodiment 2
[0031] Its technical scheme is: low-temperature vitrified bond powder 92% (volume percentage), nickel-phosphorus alloy 8%.
[0032] The raw material of low temperature vitrified bond is: silicon dioxide (SiO 2 ) 48%, alumina (Al 2 o 3 ) 6%, sodium carbonate (Na 2 CO 3 ) 6%, lithium carbonate (Li 2 CO 3 ) 5%, zirconia (ZrO 2 ) 2%, clay (Hydrotalcite) 8%, boric acid (H 3 BO 3 ) 25%.
[0033] The raw material of electroless plating solution is: nickel sulfate (NiSO 4 ) 30g / L, sodium hypophosphite (NaH 2 PO 2 ) 25g / L, sodium citrate (Na 3 C 6 h 5 o 7 2H 2 O) 25g / L, thiourea (CH 4 N 2 S) 0.001g / L.
[0034] The sintering temperature is 680°C, the pressure is 2MPa, and the pressure is held for 3min. The prepared low-temperature ceramic-metal bond has a flexural strength of 140~160MPa and an impact strength of 2.5~4kJ / m 2 , hardness 123~125HRB.
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