Preparation method of multi-functional nanometer material having good sun-proof effects
A nanomaterial and multifunctional technology, applied in the field of preparation of multifunctional nanomaterials, can solve the problems of serious photocatalytic activity, damage to cells and DNA, carcinogenicity, etc., and achieve good sun protection effect, low cytotoxicity, and large load effect
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[0033] A preparation of a multifunctional nanomaterial with better sunscreen effect, the specific operation steps are as follows:
[0034] 1) Preparation of bismuth titanate silicon spheres (BTO-DSM) with physical sunscreen properties:
[0035] At room temperature, 0.5 g of cetyltrimethylammonium bromide was added to a mixed solution containing 70 mL of water, 0.8 mL of ammonia water, 20 mL of ether and 10 mL of ethanol and stirred for half an hour. 2.5mL tetraethyl orthosilicate and 0.05mL triaminopropyltrimethoxysilane were quickly added to the above solution in sequence and continued to stir for 4 hours, and the white precipitate after the reaction was washed with water and ethanol and dried. The obtained white solid was stirred in a mixed solution of 15 mL ethanol and 105 mL hydrochloric acid at 70° C. for 1 day, washed with water and ethanol, and oven-dried at 60° C. to obtain dendritic silica microspheres (DSM).
[0036] 0.3 g of DSM and 0.128 mL of titanium tetraisopropo...
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